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Crystal structure of 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl

Authors :
V. Lakshmi Ranganatha
Vivek K. Gupta
Naresh Sharma
S. Ara Khanum
T. Prashanth
Rajni Kant
Source :
Crystallography Reports. 60:1116-1120
Publication Year :
2015
Publisher :
Pleiades Publishing Ltd, 2015.

Abstract

The title compound, 2,4,6-triisopropyl-2',5'-dimethoxybiphenyl was synthesized from 1-choloro-2.5-dimethoxy benzene, 1,3,5-triisopropylbenzene boronic acid and potassium phosphate in the presence of lead acetate as a catalyst and toluene as a solvent. Its crystal structure is determined by X-ray structure analysis. The crystals are the orthorhombic, a = 12.3281(4), b = 17.4235(5), c = 19.6550(6) A, Z = 8, sp. gr. Pbca. R = 0.0603 for 2494 observed reflections.

Details

ISSN :
1562689X and 10637745
Volume :
60
Database :
OpenAIRE
Journal :
Crystallography Reports
Accession number :
edsair.doi...........e10555beb4ec2def9d21565192a2d74c