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Studies of the effect of surface modification of carbon sorbents by poly-N-vinylpyrrolidone using a complex of physicochemical and microbiological methods
- Source :
- Protection of Metals and Physical Chemistry of Surfaces. 49:430-439
- Publication Year :
- 2013
- Publisher :
- Pleiades Publishing Ltd, 2013.
-
Abstract
- The surface of the VNIITU-1 carbon mesoporous sorbent was modified with poly-N-vinylpyrrolidone characterized by antibacterial activity. Synthesis was carried out in two stages: (1) impregnation of the carbon sorbent by an aqueous solution of poly-N-vinylpyrrolidone with the molecular mass of 10000 g/mol; and (2) impregnation of the carbon sorbent by an aqueous solution of the (N-vinylpyrrolidone) monomer and initiator with their further polymerization in an inert atmosphere. Carbon sorbent samples were studied using a complex of physicochemical methods: scanning electron microscopy, infrared spectroscopy, low-temperature nitrogen adsorption, nuclear magnetic resonance, and thermogravimetry. It was found that the polymer obtained on the carbon surface is free of the initial toxic VP monomer. Microbiological tests of modified sorbents with respect to pathogenic and opportunistic microflora were carried out.
- Subjects :
- chemistry.chemical_classification
Aqueous solution
Sorbent
Organic Chemistry
Metals and Alloys
chemistry.chemical_element
Polymer
Surfaces, Coatings and Films
Thermogravimetry
chemistry.chemical_compound
Monomer
chemistry
Polymerization
Materials Chemistry
Surface modification
Organic chemistry
Carbon
Nuclear chemistry
Subjects
Details
- ISSN :
- 2070206X and 20702051
- Volume :
- 49
- Database :
- OpenAIRE
- Journal :
- Protection of Metals and Physical Chemistry of Surfaces
- Accession number :
- edsair.doi...........f5d7fde824e227c382c20a66f80c0d7c
- Full Text :
- https://doi.org/10.1134/s2070205113040114