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Studies of the effect of surface modification of carbon sorbents by poly-N-vinylpyrrolidone using a complex of physicochemical and microbiological methods

Authors :
V. P. Talzi
A. V. Sedanova
O. N. Baklanova
V. A. Drozdov
A. N. Salanov
O. A. Knyazheva
Likholobov Vladimir A
L. G. P’yanova
Source :
Protection of Metals and Physical Chemistry of Surfaces. 49:430-439
Publication Year :
2013
Publisher :
Pleiades Publishing Ltd, 2013.

Abstract

The surface of the VNIITU-1 carbon mesoporous sorbent was modified with poly-N-vinylpyrrolidone characterized by antibacterial activity. Synthesis was carried out in two stages: (1) impregnation of the carbon sorbent by an aqueous solution of poly-N-vinylpyrrolidone with the molecular mass of 10000 g/mol; and (2) impregnation of the carbon sorbent by an aqueous solution of the (N-vinylpyrrolidone) monomer and initiator with their further polymerization in an inert atmosphere. Carbon sorbent samples were studied using a complex of physicochemical methods: scanning electron microscopy, infrared spectroscopy, low-temperature nitrogen adsorption, nuclear magnetic resonance, and thermogravimetry. It was found that the polymer obtained on the carbon surface is free of the initial toxic VP monomer. Microbiological tests of modified sorbents with respect to pathogenic and opportunistic microflora were carried out.

Details

ISSN :
2070206X and 20702051
Volume :
49
Database :
OpenAIRE
Journal :
Protection of Metals and Physical Chemistry of Surfaces
Accession number :
edsair.doi...........f5d7fde824e227c382c20a66f80c0d7c
Full Text :
https://doi.org/10.1134/s2070205113040114