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Optimization of Synthesis Conditions of LiMn2–xFexO4 Cathode Materials Based on Thermal Characterizations
- Source :
- American Journal of Analytical Chemistry. :51-59
- Publication Year :
- 2017
- Publisher :
- Scientific Research Publishing, Inc., 2017.
-
Abstract
- We have synthesized LiMn2–xFexO4 (x = 0, 0.25, and 0.50) cathode materials for applications in Li ion rechargeable batteries via sol-gel method. We studied thermal characteristics of as synthesized materials using differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). In order to optimize the synthesis conditions, we studied X-ray diffraction (XRD) of synthesized cathode materials at various temperatures, based on the transitions obtained from DSC/TGA. The XRD results can be co-related to the thermal behavior of the synthesized cathode materials and the synthesis conditions optimized.
- Subjects :
- Diffraction
Thermogravimetric analysis
Materials science
Analytical chemistry
02 engineering and technology
010402 general chemistry
021001 nanoscience & nanotechnology
01 natural sciences
Cathode
0104 chemical sciences
law.invention
Ion
Psychiatry and Mental health
Differential scanning calorimetry
law
X-ray crystallography
Thermal
0210 nano-technology
Thermal analysis
Subjects
Details
- ISSN :
- 21568278 and 21568251
- Database :
- OpenAIRE
- Journal :
- American Journal of Analytical Chemistry
- Accession number :
- edsair.doi...........fa5425bf89289c29d9e14790956f1c49