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Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy

Authors :
Yoshihide Watanabe
Noritake Isomura
Atsushi Beniya
Yusaku F. Nishimura
Tomoyuki Nimura
Satoru Takakusagi
Ryo Suzuki
Hiromitsu Uehara
Kiyotaka Asakura
Source :
Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. 34:023201
Publication Year :
2016
Publisher :
American Vacuum Society, 2016.

Abstract

A portable ultrahigh-vacuum sample storage system was designed and built to investigate the detailed geometric structures of mass-selected metal clusters on oxide substrates by polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy (PTRF-XAFS). This ultrahigh-vacuum (UHV) sample storage system provides the handover of samples between two different sample manipulating systems. The sample storage system is adaptable for public transportation, facilitating experiments using air-sensitive samples in synchrotron radiation or other quantum beam facilities. The samples were transferred by the developed portable UHV transfer system via a public transportation at a distance over 400 km. The performance of the transfer system was demonstrated by a successful PTRF-XAFS study of Pt-4 clusters deposited on a TiO2(110) surface.

Details

ISSN :
15208559 and 07342101
Volume :
34
Database :
OpenAIRE
Journal :
Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films
Accession number :
edsair.doi.dedup.....524c784c44393cbd79cd6fc3f59a24c6
Full Text :
https://doi.org/10.1116/1.4936344