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Portable ultrahigh-vacuum sample storage system for polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy
- Source :
- Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. 34:023201
- Publication Year :
- 2016
- Publisher :
- American Vacuum Society, 2016.
-
Abstract
- A portable ultrahigh-vacuum sample storage system was designed and built to investigate the detailed geometric structures of mass-selected metal clusters on oxide substrates by polarization-dependent total-reflection fluorescence x-ray absorption fine structure spectroscopy (PTRF-XAFS). This ultrahigh-vacuum (UHV) sample storage system provides the handover of samples between two different sample manipulating systems. The sample storage system is adaptable for public transportation, facilitating experiments using air-sensitive samples in synchrotron radiation or other quantum beam facilities. The samples were transferred by the developed portable UHV transfer system via a public transportation at a distance over 400 km. The performance of the transfer system was demonstrated by a successful PTRF-XAFS study of Pt-4 clusters deposited on a TiO2(110) surface.
- Subjects :
- Total internal reflection
X-ray spectroscopy
business.industry
Chemistry
Analytical chemistry
Synchrotron radiation
02 engineering and technology
Surfaces and Interfaces
010402 general chemistry
021001 nanoscience & nanotechnology
Condensed Matter Physics
01 natural sciences
Sample (graphics)
0104 chemical sciences
Surfaces, Coatings and Films
X-ray absorption fine structure
Computer data storage
0210 nano-technology
business
Spectroscopy
Absorption (electromagnetic radiation)
Subjects
Details
- ISSN :
- 15208559 and 07342101
- Volume :
- 34
- Database :
- OpenAIRE
- Journal :
- Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films
- Accession number :
- edsair.doi.dedup.....524c784c44393cbd79cd6fc3f59a24c6
- Full Text :
- https://doi.org/10.1116/1.4936344