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Convenient one-pot access to 2 H -3-nitrothiochromenes from 2-bromobenzaldehydes, sodium sulfide and β-nitrostyrenes
- Source :
- Organic and Biomolecular Chemistry, Organic and Biomolecular Chemistry, Royal Society of Chemistry, 2019, 17 (26), pp.6355-6358. ⟨10.1039/C9OB01060B⟩
- Publication Year :
- 2019
- Publisher :
- HAL CCSD, 2019.
-
Abstract
- An efficient synthesis of 2H-3-nitrothiochromenes via a cascade reaction was established. Starting from commercially available o-bromobenzaldehydes and β-nitrostyrenes with sodium sulfide nonahydrate as an inexpensive sulfur source, various substituted thiochromenes were synthesized with high functional group tolerance without any added transition metal catalyst or additive.
- Subjects :
- 010405 organic chemistry
[CHIM.ORGA]Chemical Sciences/Organic chemistry
Organic Chemistry
chemistry.chemical_element
010402 general chemistry
01 natural sciences
Biochemistry
Sulfur
Combinatorial chemistry
Sodium sulfide
0104 chemical sciences
Catalysis
chemistry.chemical_compound
Cascade reaction
chemistry
Transition metal
Functional group
[CHIM]Chemical Sciences
Physical and Theoretical Chemistry
SODIUM SULFIDE NONAHYDRATE
ComputingMilieux_MISCELLANEOUS
Subjects
Details
- Language :
- English
- ISSN :
- 14770520 and 14770539
- Database :
- OpenAIRE
- Journal :
- Organic and Biomolecular Chemistry, Organic and Biomolecular Chemistry, Royal Society of Chemistry, 2019, 17 (26), pp.6355-6358. ⟨10.1039/C9OB01060B⟩
- Accession number :
- edsair.doi.dedup.....6e0810847dbdc920e4ec729da87bdd0d
- Full Text :
- https://doi.org/10.1039/C9OB01060B⟩