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Carbon-TiO2 Nanostructures: Flame Synthesis and Characterization

Authors :
Andrea D’Anna
Gianluigi De Falco
Paola Pedata
Mario Commodo
Patrizia Minutolo
De Falco, G.
Commodo, M
Pedata, Paola
Minutolo, P
D’Anna, A.
Source :
2014 MRS Fall Meeting abd exhibit, Boston USA, November 30-December 5, info:cnr-pdr/source/autori:Gianluigi De Falco, Mario Commodo, Paola Pedata, Patrizia Minutolo, Andrea D'Anna/congresso_nome:2014 MRS Fall Meeting abd exhibit/congresso_luogo:Boston USA/congresso_data:November 30-December 5/anno:2014/pagina_da:/pagina_a:/intervallo_pagine, Materials Research Society symposia proceedings 1747 (2015). doi:10.1557/opl.2015.195, info:cnr-pdr/source/autori:Gianluigi De Falco, Mario Commodo, Paola Pedata, Patrizia Minutolo, Andrea D'Anna/titolo:Carbon-TiO2 Nanostructures: Flame Synthesis and Characterization/doi:10.1557%2Fopl.2015.195/rivista:Materials Research Society symposia proceedings/anno:2015/pagina_da:/pagina_a:/intervallo_pagine:/volume:1747
Publication Year :
2014

Abstract

The synthesis of pure titania and carbon-titania nano-powders in a premixed atmospheric fuel-rich flame was studied. The variation of the flame C/O ratio allows to produce both pure titania and carbon-TiO2 nanoparticles. Raman Spectroscopy, X-ray Diffraction, Atomic Force Microscopy, Electrical Low Pressure Impactor and Scanning Electron Microscopy were used to characterize the synthesized nano-powders, in terms of crystallinity, phase content, size and morphology. Produced nano-powders with a dimension of 25-40 nm are composed by both rutile and anatase phases, with rutile being the predominant one. Reactive Oxygen Species analysis performed on the synthesized nano-powders showed that the inclusion of carbon in the nano-powders results in a reduced adverse health effect, in terms of ROS production.

Details

Language :
English
Database :
OpenAIRE
Journal :
2014 MRS Fall Meeting abd exhibit, Boston USA, November 30-December 5, info:cnr-pdr/source/autori:Gianluigi De Falco, Mario Commodo, Paola Pedata, Patrizia Minutolo, Andrea D'Anna/congresso_nome:2014 MRS Fall Meeting abd exhibit/congresso_luogo:Boston USA/congresso_data:November 30-December 5/anno:2014/pagina_da:/pagina_a:/intervallo_pagine, Materials Research Society symposia proceedings 1747 (2015). doi:10.1557/opl.2015.195, info:cnr-pdr/source/autori:Gianluigi De Falco, Mario Commodo, Paola Pedata, Patrizia Minutolo, Andrea D'Anna/titolo:Carbon-TiO2 Nanostructures: Flame Synthesis and Characterization/doi:10.1557%2Fopl.2015.195/rivista:Materials Research Society symposia proceedings/anno:2015/pagina_da:/pagina_a:/intervallo_pagine:/volume:1747
Accession number :
edsair.doi.dedup.....772dfe0193646bef57c1d6186bffe705