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Permethylated NHC-capped aand b-cyclodextrins (ICyD Me ) Regioselective and enantioselective gold-catalysis in pure water

Authors :
Louis Fensterbank
Lise-Marie Chamoreau
Guangcan Xu
Yongmin Zhang
Xiaolei Zhu
Virginie Mouriès-Mansuy
Matthieu Sollogoub
Sylvain Roland
Olivia Bistri-Aslanoff
Institut Parisien de Chimie Moléculaire (IPCM)
Chimie Moléculaire de Paris Centre (FR 2769)
Institut de Chimie du CNRS (INC)-École normale supérieure - Paris (ENS Paris)
Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Centre National de la Recherche Scientifique (CNRS)-Ecole Nationale Supérieure de Chimie de Paris - Chimie ParisTech-PSL (ENSCP)
Université Paris sciences et lettres (PSL)-Ecole Superieure de Physique et de Chimie Industrielles de la Ville de Paris (ESPCI Paris)
Université Paris sciences et lettres (PSL)-Université Pierre et Marie Curie - Paris 6 (UPMC)-Institut de Chimie du CNRS (INC)-École normale supérieure - Paris (ENS Paris)
Université Paris sciences et lettres (PSL)-Université Pierre et Marie Curie - Paris 6 (UPMC)-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS)
Source :
Chemistry-A European Journal, Chemistry-A European Journal, Wiley-VCH Verlag, 2020, ⟨10.1002/chem.202001990⟩
Publication Year :
2020
Publisher :
HAL CCSD, 2020.

Abstract

A series of water-soluble encapsulated copper(I), silver(I) or gold(I) complexes based on NHC-capped permethylated cyclodextrins (ICyDMe ) were developed and used as catalysts in pure water for hydration, lactonization, hydroarylation and cycloisomerization reactions. ICyDMe ligands gave cavity-based high regioselectivity in hydroarylations, and high enantioselectivities in gold-catalyzed cycloisomerizations reactions giving up to 98 % ee in water. These ICyDMe are therefore useful ligands for selective catalysis in pure water.

Details

Language :
English
ISSN :
09476539 and 15213765
Database :
OpenAIRE
Journal :
Chemistry-A European Journal, Chemistry-A European Journal, Wiley-VCH Verlag, 2020, ⟨10.1002/chem.202001990⟩
Accession number :
edsair.doi.dedup.....7b690465121b993c9cd898497e12d395