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Ethyl 4-(4-cyanophenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Authors :
Zhu-Feng Li
You-Hong Zhang
De-Hong Wu
Source :
Acta Crystallographica Section E, Vol 65, Iss 8, Pp o1733-o1733 (2009), Acta Crystallographica Section E: Structure Reports
Publication Year :
2009
Publisher :
International Union of Crystallography, 2009.

Abstract

The asymmetric unit of the title compound, C15H15N3O2S, contains two independent molecules corresponding to the R and S enantiomers. The dihydropyrimidinone rings adopt a flattened boat conformation. One of the ethyl groups is disordered over two orientations with occupancy factors of 0.700 (7) and 0.300 (7). In the crystal structure, molecules are linked by intermolecular N—H...O hydrogen-bonding interactions into one-dimensional chains along the c-axis direction. The chains are further connected by N—H...S hydrogen bonds, forming a three-dimensional network.

Details

Language :
English
ISSN :
16005368
Volume :
65
Issue :
8
Database :
OpenAIRE
Journal :
Acta Crystallographica Section E
Accession number :
edsair.doi.dedup.....939a6feb3655d2115897f032c09bffbf