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Gas Ion Source Performance of the EnvironMICADAS at HEKAL Laboratory, Debrecen, Hungary
- Source :
- Radiocarbon: An International Journal of Cosmogenic Isotope Research
- Publication Year :
- 2021
- Publisher :
- Cambridge University Press, 2021.
-
Abstract
- A coupled accelerator mass spectrometer–gas interface system has been successfully operating at the Hertelendi Laboratory of Environmental Studies, Debrecen, Hungary, since 2013. Over the last 6 years more than 500 gas targets were measured below 100 µg carbon content for carbon isotopic composition. The system was tested with blanks, OxII, IAEA-C1, IAEA-C2, and IAEA-C7 standards. The performance of our instrumentation shows good agreement with other published gas-interface system data and also shows a quite good agreement with the nominal value of international standard samples. There is a measurable but quite small memory effect after modern samples, but this does not significantly affect the final results. Typical ion currents at the low energy side were between 10–15 µA with a 5% CO2 in He mixing ratio. The relative errors average ±6% for samples greater than or equal to 10 µgC sample with mean count rates of 300 counts per microgram C for OxII. The blank is comparable with other systems, which is 0.0050 ± 0.0018 F14C or 34,000–47,000 yr BP, which allows for the routine measurement of both of small environmental and archeological samples.
- Subjects :
- 010506 paleontology
Archeology
060102 archaeology
Instrumentation
Sample (material)
Analytical chemistry
chemistry.chemical_element
06 humanities and the arts
01 natural sciences
Ion source
Isotopic composition
Low energy
chemistry
Mixing ratio
General Earth and Planetary Sciences
Environmental science
0601 history and archaeology
Carbon
0105 earth and related environmental sciences
Subjects
Details
- Language :
- English
- Database :
- OpenAIRE
- Journal :
- Radiocarbon: An International Journal of Cosmogenic Isotope Research
- Accession number :
- edsair.doi.dedup.....ae0f75cfe6ec12a56ae3b3bf7a30f1ef