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Solid-state NMR study of Schiff base derivatives of 2-hydroxynaphthaldehyde. Deuterium isotope effects on 15N chemical shifts in the solid state

Authors :
Bohdan Kamieński
Zbigniew Rozwadowski
Wojciech Schilf
Source :
Magnetic resonance in chemistry : MRC. 43(7)
Publication Year :
2005

Abstract

Schiff base derivatives of 2-hydroxynaphthylaldehyde were studied by means of 13C and 15N cross-polarization magic angle spinning NMR spectroscopy and deuterium isotope effects on 15N chemical shifts, deltaN(D), in the solid state. DeltaN(D) in the solid state provided evidenced for the presence of a dynamic proton transfer equilibrium in the solid state at the room temperature.

Details

ISSN :
07491581
Volume :
43
Issue :
7
Database :
OpenAIRE
Journal :
Magnetic resonance in chemistry : MRC
Accession number :
edsair.doi.dedup.....c3bc8950d7998f382bdd523551d90e9f