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Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction
- Source :
- Chemical Communications. 56:8743-8746
- Publication Year :
- 2020
- Publisher :
- Royal Society of Chemistry (RSC), 2020.
-
Abstract
- Time-resolved mechanochemical cocrystallisation studies have so-far focused solely on neat and liquid-assisted grinding. Here, we report the monitoring of polymer-assisted grinding reactions using in situ X-ray powder diffraction, revealing that reaction rate is almost double compared to neat grinding and independent of the molecular weight and amount of used polymer additives.
- Subjects :
- In situ
Materials science
cocrystallisation
polymer-assisted grinding
010402 general chemistry
01 natural sciences
Catalysis
Reaction rate
Green Chemistry
mechanochemistry
solid-state chemistry
polymer catalyst
Materials Chemistry
chemistry.chemical_classification
010405 organic chemistry
Metals and Alloys
X-ray
General Chemistry
Polymer
0104 chemical sciences
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Grinding
Chemical engineering
chemistry
Ceramics and Composites
Powder diffraction
Subjects
Details
- ISSN :
- 1364548X and 13597345
- Volume :
- 56
- Database :
- OpenAIRE
- Journal :
- Chemical Communications
- Accession number :
- edsair.doi.dedup.....e265e27472310f65923a4010d5536553
- Full Text :
- https://doi.org/10.1039/d0cc03460f