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Which is the best 9Be carrier for 10Be/9Be accelerator mass spectrometry?

Authors :
Régis Braucher
Silke Merchel
Georg Rugel
Johannes Lachner
Helmholtz-Zentrum Dresden-Rossendorf (HZDR)
Universität Wien
Centre européen de recherche et d'enseignement des géosciences de l'environnement (CEREGE)
Institut de Recherche pour le Développement (IRD)-Aix Marseille Université (AMU)-Collège de France (CdF (institution))-Institut national des sciences de l'Univers (INSU - CNRS)-Centre National de la Recherche Scientifique (CNRS)-Institut National de Recherche pour l’Agriculture, l’Alimentation et l’Environnement (INRAE)
Source :
MethodsX, MethodsX, 2021, 8, pp.101486. ⟨10.1016/j.mex.2021.101486⟩, MethodsX, Elsevier, 2021, 5, pp.101486. ⟨10.1016/j.mex.2021.101486⟩, MethodsX, Vol 8, Iss, Pp 101486-(2021)
Publication Year :
2021
Publisher :
HAL CCSD, 2021.

Abstract

International audience; Commercial 9Be solutions used for chemical preparation of samples for accelerator mass spectrometry contain the cosmogenic long-lived radionuclide 10Be at elevated but different 10Be/9Be levels. Within a systematic study of recently produced solutions, comparison to published data and new data on customised solutions from minerals, we recommend - if no customised solution is available - the 9Be solutions from Australian Chemical Reagents (ACR) or from LGC. They contain 10Be/9Be at the 3.4 × 10−15 level, which is still suitable for the majority of Earth science applications, compared to customised solutions at the 10−16 level for lowest-level studies. Commercial solutions from Scharlab having different lot numbers, i.e. an identification number assigned to a particular lot of material from a single manufacturer, vary in 10Be/9Be by up to a factor of nine. Hence, it seems an advisable strategy to buy a bigger quantity of a single production batch (such as 10 × 100 ml bottles of 9Be at 1 g l−1) and have them tested once at any AMS facility before first use. • The best 9Be carrier for low-level 10Be/9Be applications is a customised one from minerals like phenakite. • The best 9Be carriers for medium- and high-level 10Be/9Be applications are currently from Australian Chemical Reagents (ACR) or from LGC. • As 9Be carriers from Scharlab of different batches (LOT) contain 10Be/9Be at different levels, it is advisable to buy a bigger number of bottles of the same LOT of commercial carriers after being identified to have reasonably low isotope ratios.

Details

Language :
English
ISSN :
22150161
Database :
OpenAIRE
Journal :
MethodsX, MethodsX, 2021, 8, pp.101486. ⟨10.1016/j.mex.2021.101486⟩, MethodsX, Elsevier, 2021, 5, pp.101486. ⟨10.1016/j.mex.2021.101486⟩, MethodsX, Vol 8, Iss, Pp 101486-(2021)
Accession number :
edsair.doi.dedup.....e81bef1628fffe3ca241bbeca257185f
Full Text :
https://doi.org/10.1016/j.mex.2021.101486⟩