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Nanofibers of cellulose bagasse from Agave tequilana Weber var. azul by electrospinning: preparation and characterization

Authors :
R. F. Dórame-Miranda
Carmen Lizette Del-Toro-Sánchez
Francisco Javier Reynoso-Marín
J. Aguilar
Enrique Márquez-Ríos
Francisco Rodríguez-Félix
Arturo Barrera-Rodríguez
Jose Antonio Aguilar
Miguel Angel Robles-García
Israel Ceja
Source :
Carbohydrate Polymers. 192:69-74
Publication Year :
2018
Publisher :
Elsevier BV, 2018.

Abstract

In this study, cellulose of bagasse from Agave tequilana Weber var. azul was extracted to elaborate nanofibers by the electrospinning technique. Fiber characterization was performed using Transmission Electron Microscopy (TEM), x-ray, Fournier Transform-InfraRed (FT-IR) spectroscopy, and thermal analysis by Differential Scanning Calorimetry-Thermogravimetric Analysis (DSC-TGA). Different diameters (ranging from 54.57 ± 0.02 to 171 ± 0.01 nm) of nanofibers were obtained. Cellulose nanofibers were analyzed by means of x-ray diffraction, where we observed a total loss of crystallinity in comparison with the cellulose, while FT-IR spectroscopy revealed that the hemicellulose and lignin present in the agave bagasse were removed. Thermal analysis showed that nanofibers exhibit enhanced thermal properties, and the zeta potential value (−32.5 mV) demonstrated moderate stability in the sample. In conclusion, the nanofibers obtained provide other alternatives-of-use for this agro-industrial residue and could have potential in various industrial applications, among these encapsulation of bioactive compounds and reinforcing material, to mention a few.

Details

ISSN :
01448617
Volume :
192
Database :
OpenAIRE
Journal :
Carbohydrate Polymers
Accession number :
edsair.doi.dedup.....feba4e6bd049362705487ff2ec8061ba
Full Text :
https://doi.org/10.1016/j.carbpol.2018.03.058