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A Novel Method of Probing the Fractional Composition of Nanosystems

Authors :
Alexander S. Kozlov
Alexandr K. Petrov
Gennady N. Kulipanov
Vladimir O. Aseyev
Source :
KONA Powder and Particle Journal, Vol 28, Iss 0, Pp 219-226 (2014)
Publication Year :
2014
Publisher :
Hosokawa Powder Technology Foundation, 2014.

Abstract

The article presents a comparison of the traditional methods to investigate the fractional composition of nanosized powders, namely atomic force microscopy (AFM), scanning electron microscopy (SEM), dynamic light scatterin, (DLS) and a new one – analysis of the aerosol products of submillimeter pulse laser ablation (SLA). As has previously been proven, biological macromolecules retain activity after ablation under submillimeter wavelengths, molecules become separated in the aerosol phase and each sort of molecules forms its own fraction of the aerosol particles. We suggest that this process is made possible as the result of influence on the hydrogen and van der Waals’ bonds, with the energies within the submillimeter range. Results of investigations on SiO2 and artificial diamond clusters using the above methods in both powder and colloid states are discussed. SLA with subsequent detection of aerosol products with the help of convenient aerosol equipment is found to be simple, fast and informative, and can act as a competitor to mass spectrometry, X-ray scattering and other methods.

Details

Language :
English
ISSN :
02884534 and 21875537
Volume :
28
Issue :
0
Database :
Directory of Open Access Journals
Journal :
KONA Powder and Particle Journal
Publication Type :
Academic Journal
Accession number :
edsdoj.163244f6e4b443fa96ff07b1685d5fe
Document Type :
article
Full Text :
https://doi.org/10.14356/kona.2010019