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N′-[5-Acetyl-3-(4-chlorophenyl)-2,3-dihydro-1,3,4-thiadiazol-2-ylidene]-5-(1H-indol-3-yl)-1-phenyl-1H-pyrazole-3-carbohydrazide dimethylformamide monosolvate

Authors :
Gamal A. El-Hiti
Bakr F. Abdel-Wahab
Emad Yousif
Mohammad Hayal Alotaibi
Amany S. Hegazy
Benson M. Kariuki
Source :
IUCrData, Vol 4, Iss 1, p x190148 (2019)
Publication Year :
2019
Publisher :
International Union of Crystallography, 2019.

Abstract

In the title solvate, C28H20ClN7O2S·C3H7NO, the main molecule consists of chlorophenyl (A), thiadiazolyl (B), pyrazolyl (C), phenyl (D) and indolyl (E) rings, with twist angles between neighbouring rings A/B, B/C, C/D and D/E of 32.6 (1), 14.8 (1), 60.8 (1) and 20.1 (1)°, respectively. The dimethylformamide solvent molecule accepts an N—H...O hydrogen bond from the indole group. In the extended structure, molecules related by 21 screw axes are stacked in the [001] direction to form columns linked by weak C—H...O interactions.

Details

Language :
English
ISSN :
24143146
Volume :
4
Issue :
1
Database :
Directory of Open Access Journals
Journal :
IUCrData
Publication Type :
Academic Journal
Accession number :
edsdoj.1a88510fe0994bdb8ad9bb4445ffaec5
Document Type :
article
Full Text :
https://doi.org/10.1107/S2414314619001482