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Synthesis and crystal structure of (2E)-1-[3,5-bis(benzyloxy)phenyl]-3-(4-ethoxyphenyl)prop-2-en-1-one

Authors :
K. R. Jeyashri
G. Logeshwari
U. Rajapandiyan
K. Sivakumar
S. Selvanayagam
H. Manikandan
K. Kaviyarasu
Source :
Acta Crystallographica Section E: Crystallographic Communications, Vol 80, Iss 9, Pp 913-915 (2024)
Publication Year :
2024
Publisher :
International Union of Crystallography, 2024.

Abstract

In the title compound, C31H28O4, the phenyl rings of the chalcone unit subtend a dihedral angle of 26.43 (10)°. The phenyl rings of the pendant benzyloxy groups are orientated at 75.57 (13) and 75.70 (10)° with respect to their attached ring. In the crystal, weak C—H...O and C—H...π interactions link the molecules. The intermolecular interactions were quantified and analysed using Hirshfeld surface analysis, which showed a breakdown into H...H (49.8%), H...C/C...H (33.8%) and H...O/O...H (13.6%) interactions with other types making negligible contributions.

Details

Language :
English
ISSN :
20569890
Volume :
80
Issue :
9
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E: Crystallographic Communications
Publication Type :
Academic Journal
Accession number :
edsdoj.1ee65a75cbc44813bc3c477cfcf7acef
Document Type :
article
Full Text :
https://doi.org/10.1107/S2056989024007552