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1-(2-Nitrophenyl)-3-phenylthiourea

Authors :
Yongqi Qin
Fangfang Jian
Mingna Jiang
Xiangyan Yang
Source :
Acta Crystallographica Section E, Vol 64, Iss 1, Pp o142-o142 (2008)
Publication Year :
2008
Publisher :
International Union of Crystallography, 2008.

Abstract

The title compound, C13H11N3O2S, was prepared by reaction of 2-nitrobenzenamine, KOH and 1-isothiocyanatobenzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak intermolecular N—H...S and C—H...S hydrogen-bonding interactions.

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
64
Issue :
1
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.29314e7b98cb4bf9a90d3ada810ac4f8
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536807063374