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2-Amino-7,7-dimethyl-5-oxo-4-[3-(trifluoromethyl)phenyl]-1,4,5,6,7,8-hexahydroquinoline-3-carbonitrile

Authors :
A. G. Mulik
D. R. Patil
Kamini Kapoor
Vivek K. Gupta
Rajni Kant
Madhukar B. Deshmukh
Source :
Acta Crystallographica Section E, Vol 69, Iss 1, Pp o105-o105 (2013)
Publication Year :
2013
Publisher :
International Union of Crystallography, 2013.

Abstract

In the title molecule, C19H18F3N3O, the dihydropyridine and cyclohexene rings both adopt sofa conformations. The five essentially planar atoms of the dihydropyridine ring [maximum deviation = 0.039 (2) Å] form a dihedral angle of 88.19 (8)° with the benzene ring. The F atoms of the trifluoromethyl group were refined as disordered over two sets of sites in a 0.840 (3):0.160 (3) ratio. In the crystal, N—H...O and N—H...N hydrogen bonds link molecules into a two-dimensional network parallel to (100).

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
69
Issue :
1
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.6372bbe8a1411cac1141af8ced47ab
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536812050684