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1,5-Bis(2-hydroxy-3-methoxybenzylidene)carbonohydrazide methanol 0.47-solvate

Authors :
Mouhamadou Moustapha Sow
Ousmane Diouf
Matar Seck
Aliou Hamady Barry
Mohamed Gaye
Source :
Acta Crystallographica Section E, Vol 70, Iss 4, Pp o423-o423 (2014)
Publication Year :
2014
Publisher :
International Union of Crystallography, 2014.

Abstract

In the title compound, C17H18N4O5·0.47CH3OH, the virtually planar (r.m.s. deviation = 0.128 Å) carbonohydrazide molecule is located on a twofold axis and conformation of its C=N bonds is E. There are short intramolecular O—H...N hydrogen bonds between the hydroxy groups and hydrazide N atoms. In the crystal, bifurcated N—H...(O,O) hydrogen bonds assemble the carbonohydrazide molecules into a three-dimensional network. There are C2 symmetric voids in this network, 47% of which are occupied by disordered methanol molecules.

Subjects

Subjects :
Crystallography
QD901-999

Details

Language :
English
ISSN :
16005368
Volume :
70
Issue :
4
Database :
Directory of Open Access Journals
Journal :
Acta Crystallographica Section E
Publication Type :
Academic Journal
Accession number :
edsdoj.7e8f6caa1394032a84968492a748e0e
Document Type :
article
Full Text :
https://doi.org/10.1107/S1600536814004802