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A Novel Dual Air-Bearing Fixed-χ Diffractometer for Small-Molecule Single-Crystal X-ray Diffraction on Beamline I19 at Diamond Light Source

Authors :
David . R Allan
Harriott Nowell
Sarah A. Barnett
Mark R. Warren
Adrian Wilcox
Jeppe Christensen
Lucy K. Saunders
Andrew Peach
Mark T. Hooper
Ljubo Zaja
Suren Patel
Leo Cahill
Russell Marshall
Steven Trimnell
Andrew J. Foster
Trevor Bates
Simon Lay
Mark A. Williams
Paul V. Hathaway
Graeme Winter
Markus Gerstel
Ron W. Wooley
Source :
Crystals, Vol 7, Iss 11, p 336 (2017)
Publication Year :
2017
Publisher :
MDPI AG, 2017.

Abstract

Herein, we describe the development of a novel dual air-bearing fixed-χ diffractometer for beamline I19 at Diamond Light Source. The diffractometer is designed to facilitate the rapid data collections possible with a Dectris Pilatus 2M pixel-array photon-counting detector, while allowing remote operation in conjunction with a robotic sample changer. The sphere-of-confusion is made as small as practicably possible, through the use of air-bearings for both the ω and φ axes. The design and construction of the new instrument is described in detail and an accompanying paper by Johnson et al. (also in this issue) will provide a user perspective of its operation.

Details

Language :
English
ISSN :
20734352
Volume :
7
Issue :
11
Database :
Directory of Open Access Journals
Journal :
Crystals
Publication Type :
Academic Journal
Accession number :
edsdoj.99b1736e1fc47bbac385fa72ff8adfc
Document Type :
article
Full Text :
https://doi.org/10.3390/cryst7110336