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Racemization free protocol for the synthesis of N-tert-butanesulfinyl ketimines
- Source :
- Journal of Organic Chemistry. Sept 17, 2010, Vol. 75 Issue 18, 6283-6285
- Publication Year :
- 2010
-
Abstract
- A general and robust racemization-free protocol is described for preparing a variety of N-tert-butanesulfinyl ketimines. The reaction progress is monitored by [super 1]H NMR by using the nonperturbing internal standard diglyme and ketimines are formed in either THF or CPME (cyclopentyl methyl ether) as solvent with heating to reflux.
- Subjects :
- Nuclear magnetic resonance spectroscopy -- Usage
Organosulfur compounds -- Chemical properties
Organosulfur compounds -- Structure
Schiff bases -- Chemical properties
Solvation -- Analysis
Tertiary butyl compounds -- Structure
Tertiary butyl compounds -- Chemical properties
Tetrahydrofuran -- Chemical properties
Biological sciences
Chemistry
Subjects
Details
- Language :
- English
- ISSN :
- 00223263
- Volume :
- 75
- Issue :
- 18
- Database :
- Gale General OneFile
- Journal :
- Journal of Organic Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- edsgcl.238531181