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Structure change associated with the [[M.sup.II/III] 1,4,7-triazacyclononane-N,N',N''-triacetate (TCTA)]?/0 electron transfers (M = Mn, Fe, and Ni): crystal structure for [[Fe.sup.II][([H.sub.2]O).sub.6]][[[Fe.sup.II](TCTA)].sub.2]