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Obtaining proton chemical shifts and multiplets from several 1D NMR signals

Authors :
Mandelshtam, V.A.
Van, Que N.
Shaka, A.J.
Source :
Journal of the American Chemical Society. Nov 25, 1998, p12161, 2 p.
Publication Year :
1998

Abstract

A new method of computing 1D projections from a 2D time-domain signal is reported. This uses a new numerical method extending the filter diagonalization method (FDM). This results in a decoupled-proton spectrum and an estimate of the corresponding multiplet for each decoupled signal. It avoids problems with 2D line shapes and time-frequency uncertainties, and good results are achieved with just four t1 increments.

Details

ISSN :
00027863
Database :
Gale General OneFile
Journal :
Journal of the American Chemical Society
Publication Type :
Academic Journal
Accession number :
edsgcl.53509187