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An Inversion Recovery NMR Kinetics Experiment
- Source :
-
Journal of Chemical Education . May 2011 88(5):665-669. - Publication Year :
- 2011
-
Abstract
- A convenient laboratory experiment is described in which NMR magnetization transfer by inversion recovery is used to measure the kinetics and thermochemistry of amide bond rotation. The experiment utilizes Varian spectrometers with the VNMRJ 2.3 software, but can be easily adapted to any NMR platform. The procedures and sample data sets in this article will enable instructors to use inversion recovery as a laboratory activity in applied NMR classes and provide research students with a convenient template with which to acquire inversion recovery data on research samples. (Contains 1 table, 1 scheme, and 3 figures.)
Details
- Language :
- English
- ISSN :
- 0021-9584
- Volume :
- 88
- Issue :
- 5
- Database :
- ERIC
- Journal :
- Journal of Chemical Education
- Publication Type :
- Academic Journal
- Accession number :
- EJ936780
- Document Type :
- Journal Articles<br />Reports - Descriptive
- Full Text :
- https://doi.org/10.1021/ed1006822