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Time-dependent response of treated and untreated plywood to various modes of water exposure was studied. Treatments included 1.3-dimethylol-4.5-dihydroxyethyleneurea (DMDHEU) and phenol-formaldehyde (PF). The effect of thermal modification was also investigated. Water exposure regimes included: one-sided water spray, one-sided water soak, and high humidity – all for a duration of 192 h. Direct measurements of dimensional change were recorded, and digital image correlation (DIC) was used to continuously monitor two-dimensional swelling. Over 90% of thickness swell occurred during the first 24 h of liquid water exposure. Swelling was still progressing under 90% relative humidity exposure after 192 h. DMDHEU and PF were statistically equivalent and improved thickness swell by 64% and 60%, for water spray and water soak, respectively. Chemical treatment improved thickness swell by approximately 41% under high humidity. Thermal modification improved thickness swell by 36%, 28%, and 28% for water spray, water soak, and high humidity exposure after 192 h, respectively. DIC measurements during the first 3 h of exposure revealed the fastest rate of thickness swell occurred with one-sided water spray and the slowest rate during one-sided water soak. Overall, PF-treated plywood exhibited the best initial water resistance. After 24 h DMDHEU and PF were equally effective treatments. [ABSTRACT FROM AUTHOR]

Naturally durable wood species such as western juniper (Juniperus occidentalis) are a potential source of bio-based wood preservatives for the improvement of non-durable timber species. This research investigated the durability of southern yellow pine (Pinus sp.) and western juniper lumber or strandboard. Single layer panels were made with six different types of wood or wood treatments: southern yellow pine, mixed juniper sapwood and heartwood, sapwood, heartwood, sapwood strands impregnated with juniper oil prior to and after panel manufacturing. Panels were fabricated with 560 kg/m3 oven-dry density with 5% of PF resin and 0.5% of wax. Durability testing was performed with the brown rot fungi Gloeophyllum trabeum and Rhodonia placenta and the white rot fungus Trametes versicolor. Internal bond as a crucial parameter of OSB was measured. Tests revealed that juniper heartwood and juniper heartwood strandboards were highly decay resistant, and juniper oil pre- and postimpregnation strandboard manufacture imparted increased resistance to decay against one brown rot fungus, Gloeophyllum trabeum. Juniper strandboard manufactured from non-impregnated strands showed significantly higher internal bond than pine. These results suggest there is excellent potential for manufacturing highly decay-resistant OSB from juniper, especially from heartwood and that juniper oil can increase the durability of juniper sapwood strandboard. [ABSTRACT FROM AUTHOR]

This work investigated the feasibility of using western juniper (Juniperus occidentalis) as a material to manufacture oriented strandboard (OSB) panels. Four different material combinations of juniper sapwood, heartwood, and fibrous bark were compared with regular southern yellow pine (Pinus sp.) strands. The OSB panels were made at an oven-dry density of 560 kg/m3. One pine control panel was also made at a higher density of 650 kg/m3 with a 5% addition of phenol formaldehyde (PF) resin and a 0.5% addition of wax. The single-layer panels were formed with a hot press, and the physical and mechanical properties were tested according to the ASTM standard D1037 (2020). The testing indicated that western juniper is a potential material for manufacturing of OSB panels. The properties of the juniper panels were equivalent or slightly better than those of the southern yellow pine panels at the same density level, except for the modulus of elasticity (MOE). The lower density of the juniper OSB panels may have benefits in construction applications and can decrease transportation costs. [ABSTRACT FROM AUTHOR]

Thermo-hydro-mechanical (THM) processing can improve the intrinsic properties of wood, produce new materials, and give desired form and function to new applications. THM treatments change the mechanical properties of wood and may change its viscoelastic properties as well. Therefore, the objective of this study was to assess the viscoelastic properties of THM-treated wood at several humidity and load levels. To explore these changes, this study applied a THM treatment to beech (Fagus sylvatica L.) wood with steam (620 kPa) and heat (170 °C), followed by densification and increased temperature (200 °C) in a hot-press, which was then cooled while under pressure. Two initial specimen thicknesses before THM treatment were used to study the difference between density ratios. Specimens were tested in a humidity-controlled dynamic mechanical analyser (DMA) to apply creep stress with different loading levels (20% and 30% of expected modulus of rupture) and relative humidity levels (30%, 50%, and 65% RH). The creep compliance/recovery response was monitored, and dynamic moduli were measured before and after the application of creep stress. The loss modulus measured was highest for specimens tested at 65% RH and lowest in specimens tested at 30% RH, which is a direct result of the viscous response of the material. Increased damping of the specimens was also observed at higher RH, which is typical for wood products due to added moisture in the cell wall acting as a plasticizer to cell wall polymers. Like previous studies, THM treatment lowered the equilibrium moisture content (EMC) of densified wood specimens, which affected their mechanical performance. THM treatment yields higher strength and lower EMC, suggesting that this product could be suitable for structural applications where their service life is in an indoor environment. THM treatment also resulted in decreased creep compliance and recovery compliance as compared to control specimens. [ABSTRACT FROM AUTHOR]

Grape cane is a necessary annual by-product of a vineyard. It is available in large quantities, an estimated 9 million tons (oven-dry weight) annually, having approximately 18 million acres worldwide. There is currently no substantial commercial utilization of grape cane fiber, with the majority incinerated. The main objective of the current study is to characterize grape cane fibers extracted at different alkali treatment concentrations and to determine the optimum treatment concentrations that can produce better fiber properties. The fibers were treated at 1, 3, 5 and 7 wt% of sodium hydroxide (NaOH) at 100 °C for 2 h. The grape cane fibers can be categorized into two types, namely outer bark (OB) and inner bark (IB) fiber after the treatment process. Aspect ratio, chemical composition, crystallinity, changes in the functional groups using FTIR, and tensile properties of OB and IB fibers were investigated. The results show that these two fibers demonstrated dissimilar anatomical structures, cell types, cell dimensions, and tensile properties. Meanwhile, the chemical compositions and crystallinity are equivalent to each other. The overall properties of both fibers were found superior at the lower treatment concentrations. [ABSTRACT FROM AUTHOR]

The purpose of this paper was to analyze the effects of various OSB-strand modifications on physical and mechanical properties of strand board. Norway spruce (Picea abies L. Karst) strands were acetylated using acetic anhydride or thermally modified at 180 °C using atmospheric pressure and superheated steam environment. Strand boards made of acetylated strands (Acet), thermally modified strands (TM) and thermally modified strands used only at surface layers (TMSL) were produced. Furthermore, strand boards with 20% (Cork20%) and 40% (Cork40%) cork particles were manufactured. Wood-water relations, i.e., equilibrium moisture content (EMC), water absorption (WA), thickness swelling (TS), as well as mechanical properties, i.e., bending strength and internal bonding, were tested and compared to untreated reference strand board. The EMC for TMSL was no different than the reference boards, however, the other boards had a statistically significant decrease in EMC. Acetylated strand board and boards with cork particles had a significant increase in water resistance. The mechanical properties decreased for TM and Cork40%, but no difference was shown for Cork20%. Acetylation increased internal bond strength. The results provide a comparison between different modifications of strand boards and show a new possibility of reducing the water effects on OSB with cork particles. [ABSTRACT FROM AUTHOR]

Wood structural panels are commonly subjected to short-term accelerated weathering (AW) procedures to determine relative moisture durability for quality control and product development purposes. The panel edges contribute heavily to moisture uptake since edges represent the least resistant pathway for moisture intrusion. In full-size panels, the edge area to total surface area ratio is small, and moisture intrusion is primarily limited to panel faces. When small specimens are used, such as those in AW procedures, the ratio of edge area to total surface area increases and moisture intrusion at the edges may dominate, which is referred to as the edge effect. The purpose of this study was to determine if physical and mechanical properties of oriented strand board (OSB) and plywood after AW are influenced by specimen size. Specimen width was varied while thickness and length remained constant to understand if edge effects were present in small specimens with different edge area to total surface area ratios. Three AW procedures were evaluated to determine if the effect of specimen size depends on weathering method. No clear effect of specimen size on physical and mechanical properties of either composite type was found. Differences in flexural properties between specimen widths were observed for unweathered OSB, but similar property retention between specimen widths after AW indicated the same trend as the unweathered control. Plywood results were influenced by natural defects, resulting in high variability and absence of statistically significant differences. Lateral nail resistance connection properties of both OSB and plywood were highly variable for all treatment groups and were unaffected by weathering. [ABSTRACT FROM AUTHOR]

The quality of wood composites is dependent on the bondlines' performance and their moisture resistance. The effect of moisture intrusion into bondlines is the focus of this study. The strain profile in the bondline during loading was investigated and the effects of weathering on the bondline were quantified by digital image correlation (DIC), while load deflection data were collected from lap-shear tests (LShTs). A total of 75 LShTs were evaluated including four different adhesive types with Douglas-fir wood, out of which 39 served as controls and 36 as substrates for weathering. The effect of weathering on failure load was not statistically significant. Only the bonded surface and adhesive type have significant effects on failure load, as well as the three-way interaction between the bonded surface, adhesive, and weathering, as revealed by three-way analysis of variance (ANOVA). The average effective shear moduli for the weathered samples were significantly lower than those for the control samples. [ABSTRACT FROM AUTHOR]

Technical advancements in the field of capacitive sensing and the availability of multi-channel capacitance-to-digital converters have led the way for improved sensing capabilities in the field of wood moisture content. A four-channel, planar capacitance sensor was developed and calibrated on maple veneers. The calibration material was conditioned to equilibrium at three different relative humidity levels. Optimal penetration depths were determined statistically and analytically. A rule of mixture approach and a volumetric model were applied to derive the moisture content at distinct layers. Different levels of discrepancy of the fit were observed among and within the different electrodes and calibration datasets. The sensor was able to determine changes in moisture content and positive moisture content gradients, rather than averages, with the limitation of detecting negative moisture gradients. [ABSTRACT FROM AUTHOR]

In the present study, fast-grown western hemlock (Tsuga heterophylla) was subjected to a thermal-hydro-mechanical (THM) treatment. Bond-line shear strength and durability were evaluated, and three parameters (substrate density, adhesive type and amount of adhesive spread) were investigated. To understand how THM processing affects bond performance, surface roughness and cell morphology of wood, before and after THM treatment, were observed. Adhesive penetration depths and patterns in untreated wood and THM-treated wood were also examined. In addition, Fourier transform infrared (FTIR) spectroscopy analysis of bond-line and microscopic observation of interphase region were conducted. Results revealed that polymeric diphenylmethane diisocyanate (PMDI) and polyurethane (PUR) had better bonding performance than phenol formaldehyde resin (PF). THM treatment improved bond durability, and THM plywood met the adhesive bond requirements of exterior plywood. THM treatment reduced surface roughness and porosity of wood. Adhesive penetration patterns were different in untreated wood and THM-treated wood and were affected by amount and type of adhesive. Pathways for adhesive flow into western hemlock were primarily tracheid lumens, ray cell lumens and the interconnecting pits. PF is the only adhesive that showed no evidence of flow via ray tissues or cell wall penetration. Since bond-line shear strength largely depends upon the weakest link across the laminas, ultimate strength or percent wood failure does not always depend merely on adhesive penetration. In addition, FTIR analysis showed different chemical reactions and bonding mechanisms, which provides a possible explanation of THM-caused changes in bonding performance at the molecular level. [ABSTRACT FROM AUTHOR]

The bondability/glueability of aged and sanded thermo-hydro-mechanically (THM) densified beech wood ( Fagus sylvatica L.) was tested and compared with undensified sanded beech wood as a control. THM and control specimens were bonded with five different soy protein isolate (SPI) based adhesives. Commercial SPI powder was thermally modified in the vacuum chamber at 50 or 100 °C and pH adjusted (to pH 10.0) dispersions in water prepared at 24, 50 or 90 °C. Wettability was determined with measuring the sessile drop contact angles of water. Effective penetrations (EPs) and tensile shear strengths of THM and control specimens were determined. THM and control wood had similar wettability. Although THM wood had lower moisture content than control wood, it absorbed the water more slowly than control wood. THM specimens showed lower EPs than control specimens when comparing individual adhesives due to increased density of THM wood. Adhesives prepared with SPI thermally modified at 50 °C showed statistically significantly lower tensile shear strength of bonded THM specimens than that of bonded control specimens. THM densification had no significant effect on the bonding strengths of adhesives prepared with non-modified SPI and SPI thermally modified at 100 °C. [ABSTRACT FROM AUTHOR]

Spruce ( Picea abies L. Karst) wood lamellae, thermally treated at 170, 190, 210 and 230 °C were surface densified by compression at a temperature of 150 °C to three degrees of compression. Immediate springback, set recovery, mechanical properties in 3-point flexure, Brinell hardness and density profiles measurements were used to determine the effect of thermal treatment on the properties of surface densified wood. The highest immediate springback occurred in wood specimens thermally treated at the highest temperature (230 °C) and decreased with decreasing thermal treatment temperature. The untreated samples had the highest set recovery, which decreased with the temperature of thermal treatment. The surface densification increased hardness and bending strength. The highest increase was in the case of untreated wood and decreased with the temperature of thermal treatment. The modulus of elasticity (MOE) and modulus of rupture (MOR) of surface densified wood decreased with increasing thermal treatment temperature. The trend was similar for specimens which were thermally treated but not surface densified. Surface densification increased the density of the specimens in the first few millimetres below the surface. The highest density was achieved in untreated specimens and the lowest in specimens thermally treated at the highest temperature. [ABSTRACT FROM AUTHOR]

Green building practices have created an opportunity for the forest products industry to become a leader in the creation of in- novative building products derived from renewable materials. In other industries, sandwich composites have proven to be efficient structures by meeting structural demands of traditional panel products while consuming less material. A prototype molded-core sandwich panel made of span-rated oriented strand board (OSB) facings and a bidirectional molded wood-strand core was produced. Critical mechanical properties were evaluated to determine the feasibility of this product for use in building applications. The goals of this study were to generate details on structural performance of the product, validate the design, and provide suggestions for future product development. Results indicate that this molded-core panel performs particularly well in flexure while connection properties had the largest scope for improvement. Sufficient performance was observed to validate the design, warranting production and testing of panels sized for end-use. Future product development should explore different connection systems, perform detailed engineering analyses of the mechanical properties necessary for complete structural design, and characterize physical properties of the panel. [ABSTRACT FROM AUTHOR]

Microscale X-ray computed tomography (XCT) is discussed as a technique for identifying 3D adhesive distribution in wood-adhesive bondlines. Visualization and material segmentation of the adhesives from the surrounding cellular structures require sufficient gray-scale contrast in the reconstructed XCT data. Commercial wood-adhesive polymers have similar chemical characteristics and density to wood cell wall polymers and therefore do not provide good XCT attenuation contrast in their native form. Here, three different adhesive types, namely phenol formaldehyde, polymeric diphenylmethane diisocyanate, and a hybrid polyvinyl acetate, are tagged with iodine such that they yield sufficient X-ray attenuation contrast. However, phase-contrast effects at material edges complicate image quality and segmentation in XCT data reconstructed with conventional filtered backprojection absorption contrast algorithms. A quantitative phase retrieval algorithm, which isolates and removes the phase-contrast effect, was demonstrated. The article discusses and illustrates the balance between material X-ray attenuation and phase-contrast effects in all quantitative XCT analyses of wood-adhesive bondlines. [ABSTRACT FROM AUTHOR]

The importance of adhesion in production of wood-based composites is well-known. Adhesive penetration and interphase morphology play an important role in bond strength and product performance. Many studies offered different methods for interphase characterization and analysis. Both qualitative and quantitative methods have been used to analyze the bondline. Most of the quantitative methods were developed for bonded assemblies of veneer or wood blocks. Adhesive penetration measurement in particulate wood-based composites is the main scope of this study. For this purpose, uniform oriented strand board with veneer strands was produced by the use of phenol formaldehyde resin with 2, 6, and 10 % strand moisture content (MC). The strands were formed into well-organized mats to achieve a uniform structure for the composite. Cross-section specimens were prepared from each board and observed by epifluorescence microscopy. Six positions for growth-ring angle in adhesive joints were denoted to evaluate penetration in different directions of the wood. Four parameters were also determined to quantify resin penetration patterns by counting the quantity of the main anatomical elements of wood, which were filled with resin. Finally, it was determined that this method could recognize the differences between adhesive penetration in boards produced with different level of strand MC. Resin penetration in strands with 6 and 10 % MC was the greatest. Growth-ring angle of the strands influenced penetration as it was increased when both strands meet each other in an oblique position, although this effect was significant only in maximum penetration depth in fibers. [ABSTRACT FROM AUTHOR]

Compression creep experiments of Douglas-fir wood (Pseudotsuga menziesii) were performed at high temperature (150°C, 160°C, and 170°C) and under various conditions of steam pressure. The results established that environment conditions had a significant effect on compressive deformation, with the largest deformation obtained under saturated steam conditions. While the temperature significantly affected the compressive deformation of specimens under transient conditions, the temperature within the range studied had little effect on the compressive deformation in saturated steam. Furthermore, in specimens compressed under superheated and transient steam conditions, primary creep behavior was exhibited; while in specimens compressed under saturated steam conditions, creep deformation appeared to enter directly into secondary creep. Moreover, in saturated steam specimens very little creep was observed due to high initial deformation and little potential for additional cell wall buckling. The compressive creep measurements of Douglas-fir were compared with compressive creep of hybrid poplar (Populus deltoides×Populus trichocarpa). Due to lower initial density, and perhaps smaller microfiber angle and lower lignin content of tension wood, the compressive creep modulus of hybrid poplar was lower than Douglas-fir. Therefore, compressive deformation of Douglas-fir, at nearly all examined steam conditions and temperatures, was smaller than compressive deformation of hybrid poplar. [ABSTRACT FROM AUTHOR]

In this study, birch ( Betula pendula L.) veneers were simultaneously densified and dried using a contact drying method at pressures of 1.5 and 3 MPa at 130 °C and compared with veneer dried in a laboratory-scale convective type dryer. Compression rate, thickness swelling, and the density profiles of the veneers were investigated. Furthermore, the microstructure of densified veneers was studied by scanning electron microscopy (SEM). A maximum veneer compression rate of 9 % was achieved at a pressure of 3 MPa. Under these conditions, the veneers were, on average, densified from 504 to 574 kg m (approximately 14 %). After water soaking, full set-recovery-recovery to the initial thickness-occurred. However, the swelling rate was lower for the densified veneer. Density profiles measurements showed that densification occurs throughout the veneers. The SEM images showed that the surface of the densified veneers were smoother, whilst no cracks were detected due to densification. Densification seemed to occur in vessels. Typically, rays were bent when there was a vessel nearby. [ABSTRACT FROM AUTHOR]

Viscoelastic thermal compression (VTC) is a type of thermal-hydro-mechanical (THM) processing that requires only a short processing time. THM processing causes some chemical transformations, the nature and extent of hydro-thermolysis depends on the special treatment conditions and the chemical nature of wood species. In the present study, the chemical transformations of the cell wall components and wood extractives during VTC treatment were investigated, and correlation between chemical characterizations and observed property changes was analyzed. For this purpose, the content of extractives and pH values were determined, and FTIR analysis was performed on extractable substances, extract-free wood, holocellulose, α-cellulose and lignin. Two temperatures and two steam exposure times were adopted to determine the influence of processing conditions on chemical characterization of Tsuga heterophylla. The results revealed that THM treatment caused a series of chemical reactions in extractives. Treatment temperature and conditioning time have significant influence on chemical changes of extractives. For all of the VTC treatments used in this study, no significant changes occurred in the lignin and α-cellulose components. The only significant chemical changes occurred in the hemicelluloses, which were primarily reduction of carbonyl and acetyl functional groups. This study also confirmed that the chemical transformation of wood correlates with property changes of VTC wood. [ABSTRACT FROM AUTHOR]

A phenol formaldehyde (PF) adhesive was uniformly tagged with iodine such that it yielded sufficient X-ray computed tomography (XCT) gray-scale contrast for material segmentation in reconstructed wood-composite bondlines. Typically, untagged adhesives are organic and have a similar solid-state density as wood cell-walls, and therefore cannot be segmented quantitatively in XCT data. The iodinated PF development involved analysis and comparison of three trial adhesives containing rubidium, bromine, or iodine. Adhesive tag efficacy was measured in terms of X-ray absorption contrast enhancement and tag uniformity along the adhesive polymers. Cured adhesive density, tag element, and concentration were each found to significantly impact XCT contrast results, which in turn agreed with theoretical X-ray attenuation predictions for each resin. Ion chromatography confirmed the absence of free iodide in the liquid PF prior to bonding, and fluorescence microscopy and energy-dispersive spectroscopy (EDS) showed that iodine tags remained associated with the cured adhesive polymers. XCT and EDS results also demonstrated that when contrast agents are simply mixed into resins, rather than attached to the polymer chains, they are free to migrate independent of the penetrating adhesives during bonding. This then can cause complications with quantitative segmentation and analyses. The iodinated PF yielded consistent and uniform XCT gray-scale contrast; its formulation could be adjusted for other viscosity or molecular weight distribution, which would affect its penetration behavior. [ABSTRACT FROM AUTHOR]

Hybrid poplar ( Populus deltoides × Populus trichocarpa) and Douglas-fir ( Pseudotsuga menziesii) wood specimens were densified with three variations of thermo-hydro-mechanical (THM) treatment. The THM treatments differed in the steam environment, including transient steam (TS), saturated steam (SS), and saturated steam with 1-min post-heat treatment at 200 °C (SS+PHT). The bending properties, FTIR spectra, and colour of the THM wood specimens were studied before and after exposure to two different wood decay fungi, brown rot Gloeophyllum trabeum, and white rot Trametes versicolor. The results showed that the performance of densified hybrid poplar wood was considerably poorer than the performance of Douglas-fir heartwood. The FTIR spectra measurements did not show changes in the densified hybrid poplar wood, while some changes were evident in densified Douglas-fir specimens. After fungal degradation, the most prominent changes were observed on the SS+PHT specimens. Colour is one of the most important parameter predominantly influenced by the wood species and the intensity of the densification process for both wood species, while after fungal exposure, the colour of all densified Douglas-fir specimens obtained more or less the same appearance, and densified hybrid poplar specimens resulted in lighter colour tones, indicating that the pattern of degradation of the densified and non-densified specimens are similar. The 3-point bending test results determined that the THM treatment significantly increased the modulus of rupture (MOR) and modulus of elasticity (MOE) of the densified wood specimens, while fungal exposure decreased the MOE and MOR in hybrid poplar and Douglas-fir specimens. [ABSTRACT FROM AUTHOR]

Copyright of European Journal of Wood & Wood Products / Holz als Roh- und Werkstoff is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Copyright of European Journal of Wood & Wood Products / Holz als Roh- und Werkstoff is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Copyright of European Journal of Wood & Wood Products / Holz als Roh- und Werkstoff is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Copyright of European Journal of Wood & Wood Products / Holz als Roh- und Werkstoff is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

The paper describes for the first time the analysis of the structure of compressed wood using computed tomography. The anatomical structures of Douglas-fir and hybrid poplar before and after densification with the viscoelastic thermal compression (VTC) process were described by pore size distributions and mean pore sizes and compared. The compression of Douglas-fir mainly affected earlywood, while the compression of hybrid poplar mainly occurred in the vessels. In both wood species, the densification resulted in a significant decrease in the pore volumes. The porosity decreased to less than half of the original value for Douglas-fir earlywood and to approximately one-quarter for the vessels in hybrid poplar. The relevant mean pore sizes also decreased dramatically to about one-quarter compared to the original values. In contrast, latewood in Douglas-fir and libriform fibers in hybrid poplar are quite stable under compression. Douglas-fir latewood retained its original structure after compression and did not show any reduction in pore size. The results confirmed that the anatomical structure of VTC densified wood can be described by pore size distributions and mean pore sizes. However, in the case of broad or bimodal distributions, the mean pore sizes are of less significance. [ABSTRACT FROM AUTHOR]

Low-density hybrid poplar wood ( Populus deltoides × Populus trichocarpa) was densified by mechanical compression under saturated steam, superheated steam, and transient conditions at temperature levels of 150, 160, and 170°C. Furthermore, compression of wood under saturated steam conditions at 170°C, followed by post-heat-treatment at 200°C for 1, 2, and 3 min, was performed. To determine the influence of compression treatment on the set recovery, specimens were subjected to five cycles of water soaking and drying. Modulus of rupture (MOR) and modulus of elasticity (MOE) of specimens compressed under saturated steam conditions at 170°C and post-heat-treated at 200°C were determined in the dry condition and after five soak/dry cycles. Higher temperature of the compression treatment resulted in lower equilibrium moisture content, while the steam conditions during the treatment and the post-heat-treatment did not have significant effect. Furthermore, the highest degree of densification was obtained in specimens compressed under saturated steam conditions at 170°C and post-heat-treated at 200°C. The steam condition and temperature influenced the set recovery of compressive deformation. Reduced hygroscopicity does not necessarily imply reduced set recovery. The results established that considerable fixation of compressive deformation can be obtained by compressing the wood in a saturated steam environment and by post-heat-treatment at 200°C. The short heat-treatment had no influence on MOR or MOE, but soaking/drying treatments caused a decrease in the MOR and MOE. [ABSTRACT FROM AUTHOR]

In this paper, the compressive deformation of hybrid poplar wood ( Populus deltoides × Populus trichocarpa) at high temperature (150, 160, and 170°C) and under various conditions of steam pressure was studied. Temperature and conditions of steam environment affected the relative density change and creep deformation during compression, as well as properties of the resulting densified material. While the temperature significantly affected the compression deformation of specimens compressed under transient and superheated steam conditions, temperature within the range studied had little effect on the compressive deformation in saturated steam. In all tested conditions, compression deformation was achieved without cell wall fractures. Higher temperature of compression, regardless of steam condition, resulted in lower equilibrium moisture content. In specimens compressed under saturated steam, the modulus of rupture (MOR) and modulus of elasticity (MOE) were increased proportionally to the increase in density, while the compression under superheated steam produced lower increase in the MOE and MOR than expected based on the increase in density. Compression in transient steam conditions at 170°C produced densified wood with higher MOE and MOR than expected based on the increase in density. [ABSTRACT FROM AUTHOR]

Purpose – This paper describes a practical approach to implement computational steering for problem solving environments (PSEs) by using WBCSim as an example. WBCSim is a Web based simulation system designed to increase the productivity of wood scientists conducting research on wood-based composites manufacturing processes. WBCSim serves as a prototypical example for the design, construction, and evaluation of small-scale PSEs. Design/methodology/approach – Various changes have been made to support computational steering across the three layers – client, server, developer – comprising the WBCSim system. A detailed description of the WBCSim system architecture is presented, along with a typical scenario of computational steering usage. Findings – The set of changes and components are: design and add a very simple steering module at the legacy simulation code level, provide a way to monitor simulation execution (alert users when it is time to steer), add an interface to access and visualize simulation results, and perhaps to compare intermediate results across multiple steering attempts. These simple changes and components have a relatively low cost in terms of increasing software complexity. Originality/value – The novelty lies in designing and implementing a practical approach to enable computational steering capability for PSEs embedded with legacy simulation code. [ABSTRACT FROM AUTHOR]

Density profile relation to hardness of VTC wood composites was evaluated using X-ray densitometry and modified Brinell hardness method using different applied forces. Moreover, surface elasticity was evaluated. Prior to lamination, the low-density hybrid poplar ( Populus deltoides × Populus trichocarpa L.) and Douglas-fir ( Pseudotsuga menziesii L.) thin boards were compressed to 1.22 or 1.14 g/cm, respectively. Two different kinds of laminations were made, either single layer of 1.5 mm thickness or two 1.5-mm layers bonded to unmodified wood. The results show that thicker laminate has a great positive influence on Brinell hardness. This study suggests that results from the existing method for Brinell hardness are not comparable, and if applied force is chosen without restraint, the effect on the hardness value is significant for inhomogeneous wood composites. [ABSTRACT FROM AUTHOR]

Compression creep experiments of hybrid poplar (Populus deltoides×Populus trichocarpa) were performed in a pressurized vessel equipped with a heated hydraulic press. The viscoelastic response at various stress levels (2-7 MPa), a temperature of 170°C and transient steam conditions was studied. Moisture content and oven-dry density of compressed specimens were determined. While some recovery of compression strain occurred, compression resulted in permanent deformation and increased wood density. The influence of stress level on the amount of set recovery of compressive deformation was evaluated after 24 h water soaking. Applied stress level had a significant effect on the compression deformation. The initial strain, as well as creep strain, varied depending on the applied stress level. The highest oven-dry density was obtained at a stress level of 6.9 MPa. Lower stress levels resulted in lower moisture content after the compression process, while the equilibrium moisture content of compressed specimens was not significantly affected by stress level. Set recovery increased from 20% to 65% with increased stress level from 1.7 MPa to 4.1 MPa, then decreased to 53% for specimens compressed at 6.9 MPa. Moisture content after the compression process significantly affected the set recovery. [ABSTRACT FROM AUTHOR]

Copyright of European Journal of Wood & Wood Products / Holz als Roh- und Werkstoff is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)

Low-density hybrid poplar ( Populus deltoides × Populus trichocarpa) was densified with the viscoelastic thermal compression (VTC) process to three different degrees of densification (63%, 98%, and 132%). Durability of the VTC treated specimens was assessed by exposure to two white rot fungi ( Pleurotus ostreatus and Trametes versicolor) for four or eight weeks. After incubation, mass loss in grams and percentage mass loss were determined. The results showed that VTC densification did not change decay resistance to Pleurotus ostreatus and Trametes versicolor. The mass losses caused by Trametes versicolor were more extensive than those by Pleurotus ostreatus. As expected, longer exposure time resulted in higher mass loss. Furthermore, the degree of densification did not influence susceptibility to fungal degradation. [ABSTRACT FROM AUTHOR]

The main objective of this study was to investigate the properties of polymer composites reinforced with grape cane fibers. The fibers were subjected to a sodium hydroxide (NaOH) treatment at two treatment concentrations to extract the fibers as well as fiber surface treatment. Panels were fabricated by hand lay-up and compression molding according to different fiber types, namely outer bark (OB) and whole (W) fibers. The whole fiber was a mixture of OB and inner bark (IB) fibers. Grape cane fibers were used as the reinforcement material for unsaturated polyester (UPE) resin panels. Acrylated epoxidized soybean oil (AESO) was used as a reactive diluent material with the UPE resin, and the results were compared with panels prepared with commercial styrene–UPE. There were inconsistent alkali treatment concentration effects on the mechanical properties and water absorption. However, panels fabricated with the whole bark fibers that have been treated with 1 wt % NaOH and had AESO–UPE resin resulted in the best tensile and flexural strength. [ABSTRACT FROM AUTHOR]

A mathematical model of the hot-pressing consolidation process for manufacturing a multi-layered oriented strand composite is developed and tested. Such a process model requires independent physical properties and user-specified structure for each layer of the mat. The model uses two-dimensional (slow variation is assumed in the third dimension) heat- and mass-transfer theory and a viscoelastic compression model. The through-the-thickness (vertical) density profile (VDP) was found to be highly dependent on the initial moisture content gradient, internal mat strand properties, and hydrothermal compressive response of the mat. The VDP predicted by the model showed good agreement with experimental results. The proposed mathematical model thus shows promise as a tool to analyze optimally design-oriented strand composites. [ABSTRACT FROM AUTHOR]

A novel wood-based composite has been developed for use in structural applications. The process was designed to utilize rapidly-grown, low density, wood species. Plantation grown radiata pine is particularly well suited to this process. This is a laminated composite, where the lamina may be comprised of various materials, some of which have been treated with the viscoelastic thermal compression (VTC) process. The VTC process increases the density of wood, without causing fractures in the cell wall, thus increasing strength and stiffness of the wood material. The process may be applied to veneer, sawn wood, or strand composites. The VTC lamina is then bonded to other lamina to produce the final product. The strength and stiffness of this VTC composite exceeds any wood-based composite that is currently on the market. For example, modulus of elasticity in bending of over 20 GPa is easily obtainable. [ABSTRACT FROM AUTHOR]

Surface energy of yellow-poplar wood from three wood treatment groups was studied using sessile-drop contact-angle measurements and the Chang acid–base model for surface energy calculation. Water, glycerol, formamide, ethylene glycol and α-bromonaphthalene were used as probe liquids. Wood treatments were control, hygro-thermal treatment and densification. Contact angle trends for densified and hygro-thermally treated wood were found to be the same. Total surface energy decreased with both hygro-thermal treatment and densification. [ABSTRACT FROM AUTHOR]

Bond performance of hygro-thermally compression densified wood was studied using hygro-thermally treated and control yellow-poplar wood (Liriodendron tulipifera). Opening mode double cantilever beam fracture testing and cyclic boiling were used to evaluate bond performance. Phenol–formaldehyde (PF) film and polymeric diphenylmethane diisocyanate (pMDI) adhesives were used to bond specimens for fracture testing. Fracture toughness of hygro-thermal samples bonded with PF film was significantly higher than control samples, while no difference was found for densified samples. Fracture toughness of densified samples bonded with pMDI was significantly higher than control samples, however no change was seen for hygro-thermal samples. Cyclic boiling reduced the fracture toughness of hygro-thermal fracture samples only, irrespective of adhesive type. [ABSTRACT FROM AUTHOR]

Unlike constant moisture effects on the behavior of composite materials, transient moisture effects are not well studied and known. Armstrong and Kingston have shown that the creep of wood under transient humidity levels could be greatly accelerated over that at any constant moisture content. Later this phenomenon was termed "mechano- sorptive". In this paper, the authors show that aramid fibers (Kevlar® 29, Kevlar® 49, and Kevlar® 149) and Kevlar® 49/epoxy composites exhibit mechano-sorptive phenomenon. Kevlar® composites were studied using both creep and dynamic mechanical analysis while undergoing desorption. Creep of single Kevlar® fibers was studied during relative humid ity conditions cycled between 5 % and 95 %. The results observed with Kevlar are consis tent with those reported for other natural polymeric materials. [ABSTRACT FROM PUBLISHER]

The vertical density profile of wood-based composites is often measured using X-ray densitometry. During preliminary studies, in which the density profiles of wood composites with discrete layers of varying density were measured, it was observed that the absolute density values of the layers were incorrect when compared to gravimetric measurements of the individual layers. This is due the recommended calibration process of the X-ray densitometer, which uses the overall density of the composite to determine the X-ray attenuation factor. The severity of the error increases with the difference between minimum and maximum density in the profile. [ABSTRACT FROM AUTHOR]

Spalted wood, wood colored by fungi, has been popular in woodcraft for centuries. Most spalted wood, however, is found in an advanced state of decay and cannot be utilized. This project describes the use of viscoelastic thermal compression (VTC) to investigate the potential increase in spalted woods' strength and stiffness, with the main objective of converting so-called "punky" wood into the top layer (veneer layer or "coating") on commercial flooring. Spalted Acer macrophyllum logs were cut into veneers of size 7 mm × 7.8 cm × 25 cm and were then VTC-treated at 150 °C and 50 psi for 11.5 min. Statistical analysis on the mixed linear models showed significant increases for both the density and hardness of spalted wood (p < 0.0001). Density and Brinell hardness increased by 84% and 209%, respectively. FTIR analysis revealed that the wood polymers present in spalted wood were more susceptible to degradation imposed by the heat of the VTC treatment compared to sound wood. Additionally, the color analysis of the wood specimens showed statistically significant changes in color after the VTC treatment (p < 0.0001), which turned the wood surface darker and redder. The use of the VTC technology to transform spalted wood into wood flooring is viable. However, when exposed to moisture, the VTC-treated spalted wood showed a high percentage of set recovery (78%), which was significantly different from the set recovery of the sound wood (71%, p = 0.004). Successful use of VTC-treated spalted wood for flooring will require addressing of the swelling issue, and additional studies are needed to fully characterize the anatomy of VTC-treated spalted wood. [ABSTRACT FROM AUTHOR]

A correction to the article "The Wettability and Bonding Performance of Densified VTC Beech (Fagus sylvatica L.) and Norway Spruce ( Picea abies (L.) Karst.) Bonded With Phenol-Formaldehyde Adhesive and Liquefied Wood" that was published online on February 21, 2013 is presented.