Search

Contact experiments between low‐reactivity CaO–BaO–Al2O3‐based mold fluxes, F1 and F2, and 1.4–2.2 mass% of Al‐containing steels are conducted to investigate the effect of interfacial reaction on mold flux properties and the ultimate limit of reaction duration capacity of the developed mold flux. F1 contains 30.76% CaO, 17.03% Al2O3, 13.40% BaO, and 10.70% SiO2, whereas F2 consists of 27.90% CaO, 23.60% Al2O3, 12.90% BaO, and 9.57% SiO2 of the mass. The pre‐ and post‐experimental wettability of slag samples on steel substrates and the lubrication behavior of slags are discussed. The main results reveal that SiO2, Na2O, and B2O3 in the mold flux react with [Al] in the molten steel at steel–slag interface. The variations in slag properties indicate that both reaction durations between F1 reacting with twinning‐induced plasticity (TWIP) and F2 reacting with 20Mn23AlV steel can last for 40 min, whereas F2 has wider potential applicability for the continuous casting of Al‐containing steels. Interfacial reaction deteriorates the wettability of slag F2 on 20Mn23AlV steel substrate and reduces slag consumption, as equilibrium contact angle increases from approximately 3° to 37°, but slag consumption prediction is 0.22 kg m−2, which is likely to meet the requirement for lubrication. [ABSTRACT FROM AUTHOR]

To moderate the erosion in a slag-line zone and extend the service life of a submerged entry nozzle during continuous casting of high-Mn and high-Al steel, the current study developed a low-reaction CaO-Al2O3-based slag with lower SiO2 and higher Al2O3 contents than that of conventional CaO-SiO2-based slag. The static sessile drop technique and dynamic rotating cylinder method were utilized to investigate the erosion behavior of ZrO2-graphite refractory by the above slags. The main results indicated that silicate-based slag could wet the ZrO2-graphite substrate completely, while the aluminate-based slag spread rapidly in the first 20 minutes, and then a slag drop with an unchanged profile formed on the substrate. The equilibrium contact angles with the substrate at 1623 K were 0 and 79 deg for the CaO-SiO2 and CaO-Al2O3 based slags, respectively. The comparison of the influences of the rotating speed and the temperature revealed that the decrease of erosion rate could be realized by the developed slag. An examination of ZrO2-saturation limit also indicated that the low-reaction slag could dissolve much more ZrO2 oxidation, accompanied by a less-negative effect on the viscosity of the molten slag. [ABSTRACT FROM AUTHOR]

The complete crystallization process of mold slag in the crucible (inner diameter: 6.2 mm) was successfully recorded in situ using a digital optical microscope and image processing software in an infrared furnace (IR‐MOP). The crystallization behavior of non‐volatile mold slag tested with the new method is consistent with the findings of differential scanning calorimetry (DSC) analysis. Although the volatilization ratios of volatile mold slag during both DSC and SHTT experiments are greater than 8%, it is less than 1.2% during IR‐MOP experiments equipped with an isolated observation system, which explains why the difference in the initial crystallization temperature measured by the three methods was very large. Therefore, IR‐MOP equipped with an isolated observation system can record and accurately measure the crystallization behavior of volatile mold slag. [ABSTRACT FROM AUTHOR]

This paper presents the design, fabrication, and characterization of a middle-infrared (MIR) linear variable optical filter (LVOF) and thermopile detectors that will be used in a miniaturized mixed gas detector for CH4/CO2/CO measurement. The LVOF was designed as a tapered-cavity Fabry-Pérot optical filter, which can transform the MIR continuous spectrum into multiple narrow band-pass spectra with peak wavelength in linear variation. Multi-layer dielectric structures were used to fabricate the Bragg reflectors on the both sides of tapered cavity as well as the antireflective film combined with the function of out-of-band rejection. The uncooled thermopile detectors were designed and fabricated as a multiple-thermocouple suspension structure using micro-electro-mechanical system technology. Experimentally, the LVOF exhibits a mean full-width-at-half-maximum of 400 nm and mean peak transmittance of 70% at the wavelength range of 2.3~5 μm. The thermopile detectors exhibit a responsivity of 146 μV/°C at the condition of room temperature. It is demonstrated that the detectors can achieve the quantification and identification of CH4/CO2/CO mixed gas. [ABSTRACT FROM AUTHOR]

High frequency surface acoustic wave (SAW) technology offers many opportunities for aerospace applications in passive wireless sensing and communication. This paper presents the design, simulation, fabrication, and test of an L -band SAW resonator based on 128° Y-X LiNbO 3 substrate. The design parameters of SAW resonator were optimized by the finite element (FEM) method and the coupling-of-mode (COM) theory. Electron-beam lithography (EBL) technology was used to fabricate the submicron-scale of interdigital transducers (IDTs) and grating reflectors. The effects of some key EBL processes (e.g., the use of electron beam resist, the choice of metal deposition methods, the charge-accumulation effect, and the proximity-effect) on the fabrication precision of SAW devices were discussed. Experimentally, the LiNbO 3 -based SAW resonators fabricated using improved EBL technology exhibits a Rayleigh wave resonance peaks at 1.55 GHz with return loss about -12dB, and quality factor Q is 517. Based on this SAW resonator, the temperature and strain sensing tests were performed, respectively. The experimental results exhibit a well linear dependence of temperature/strain on frequency-shift, with a temperature sensitivity of 125.4 kHz/C and a strain sensitivity of -831 Hz/με, respectively., Competing Interests: The authors declare no conflict of interest.