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The influence of prior-β-grain (PBG) size on the tensile behavior of a laser-deposited α/β Ti–6.5Al–3.5Mo–1.5Zr–0.3Si alloy was investigated to reveal the strengthening mechanism of PBGs. Results show that the strength increases with increasing PBG size. This special coarse-PBG strengthening predominantly depends on the strong constraints resulting from the strain incompatibility among PBGs rather than PBG boundary resistance to dislocation motion. With increasing PBG size, increasing constraints are developed in the adjacent PBGs, and thus the applied stress needed to maintain the compatible deformation among these PBGs increases. In particular, the strengthening effect is not significantly affected by increasing temperature, which reveals a potential strengthening method that can strengthen a laser-deposited α/β Ti alloy at room and elevated temperatures simultaneously by controlling its PBG size. [ABSTRACT FROM AUTHOR]

The mechanical behavior of commercial purity Ti (CP-Ti)/Ti–6Al–2Zr–1Mo–1V structurally graded materials (SGMs) fabricated by laser additive manufacturing was investigated via uniaxial tensile experiments. Although the strength of all SGM specimens is higher than that of the monolithic CP-Ti specimens, only the SGM specimen of Ø10mm gauge diameter with bulky α-grains exhibits excellent plasticity comparable to the CP-Ti specimen under the same conditions. The SGM presents a potential for use as load-bearing components due to its good strength–ductility balance. [ABSTRACT FROM AUTHOR]

Abstract Under high strain rate loadings, many engineering materials exhibit quite different deformation behavior from those under quasi-static loadings, and adiabatic shear band (ASB) is normally generated with degradation of material property. In this study, the deformation response of LAMed Ti-6.5Al-3.5Mo-1.5Zr-0.3Si titanium alloy (TC11) under high strain rates (2800s−1 and 2900s−1) is investigated for both as-deposited state and heat-treated state (annealed at 1263 K for 1 h followed by annealed at 803 K for 6 h) by using the split Hopkinson pressure bar (SHPB). Results indicate that the as-deposited alloy has a unique mixed grain morphology (coarse columnar grains and fine equiaxed grains) with ultrafine basket-weave microstructure. Under high strain rate loadings, the as-deposited alloy possesses excellent yield strength but with poor plasticity and high adiabatic shear susceptibility. After heat treatment, the yield strength of alloy is sacrificed due to the reduced contents of ultrafine α lamellas, but the partially globularization of continuous grain boundary α phases greatly improves the plasticity of alloy that the adiabatic shear susceptibility is efficiently suppressed. Highlights • TC11 titanium alloy plate was fabricated by laser additive manufacture technology. • High strain rate response of the prepared alloy was investigated. • Dynamic mechanical properties corresponding to different microstructures are given. • Heat treatment efficiently suppress the adiabatic shear susceptibility of alloy. [ABSTRACT FROM AUTHOR]

The fatigue properties of the Ti-6.5Al-3.5Mo-l.5Zr-0.3Si alloy produced by direct laser deposition (DLD) have been investigated. The fatigue limit of the alloy perpendicular to and parallel to the deposition direction at specified life of 10 7 and stress ration of 0.1 is 337 MPa and 365 MPa, respectively. The porosities of specimens are among 0.014–0.028%, averaged porosity is 0.02%. The fatigue cracks initiate at the pores near the surface, which are located mostly at the column grain boundary during solidification. The size of pore and its distance from the surface are two important factors to control the fatigue life of specimen, i.e., bigger the pore or nearer to the surface, shorter the fatigue life. The fatigue fracture consists of fatigue source, radial slow crack growth and rough fast fracture region. The columnar grains boundaries of Ti-6.5Al-3.5Mo-l.5Zr-0.3Si alloy by epitaxial growth from the underlying template grains layer-by-layer during direct laser deposition are the weak joints under the cyclic stress and crack formed propagates preferentially along the grain boundaries, which should be a key factor leading to the difference of fracture morphology in the region of fatigue source and final fast fracture, and also the lower fatigue limit of specimen perpendicular to the deposition direction than that parallel to the deposition direction. [ABSTRACT FROM AUTHOR]

The near-β titanium alloy Ti-5Al-5Mo-5V-1Cr-1Fe (Ti-55511) fabricated by laser additive manufacturing was further annealed by multiple low temperature aging heat treatments. Microstructures and fracture surfaces were observed by optical and electron microscopes. Brittle tensile fracture behaviors were analyzed and cleavage fracture and quasi-cleavage fracture were distinguished. Results show that athermal ω phases in Ti-55511 have negligible strengthening effect because of their very small sizes and low content. With the aid of age hardening heat treatment, nano-scaled α phases precipitate, leading to higher microhardness. But the tensile properties of Ti-55511 did not effectively improve because brittle fracture happens due to the precipitation of nano-scaled α phases, which have similar sizes with brittle ω phases. The brittle fracture behavior is more relevant to α phase sizes instead of their volume fractions. With aging temperature increasing, the sizes of nano-scaled α phases increase and the alloy brittleness slightly decreases. [ABSTRACT FROM AUTHOR]

The near-β titanium alloy Ti-5Al-5Mo-5V-1Cr-1Fe (Ti-55511) was treated by laser surface remelting (LSR) with a series of holding times at 500 °C in order to study the growth behavior of ω-assisted α phase and its effect on mechanical properties. Transmission electron microscope and hardness test was used to characterize different phases and surface property of different samples. Results show that only a small quantity of athermal ω phases precipitate from β matrix at the remelted zone and there are incomplete collapsed {111} β lattice planes at the β/ω boundaries because Ti-55511 has low electron/atom ratio and high Al contents. So the athermal ω phase precipitated during LSR process has little effect on increasing surface hardness of Ti-55511. ω-Assisted nano-scaled α lamellas can be formed by the connection of some initial α phases at the early stage of low temperature isothermal heat treatment. And all the ω phase dissolved after 500°C/10min. Further increasing of holding times will cause volume fractions increase of the nano-scaled α lamellas, resulting in gradually improving hardness of the alloy at the remelted zone. [ABSTRACT FROM AUTHOR]

The near-β titanium alloy Ti-5Al-5Mo-5V-1Cr-1Fe (Ti-55511) was firstly remelted on the surface by laser and a series of subsequent low temperatures aging treatments were carried out to obtain ultrafine microstructures in the remelted layer. Microhardness and wear resistance of each treated sample were then tested to evaluate the effects of ω-assisted α phase on the surface properties. Microstructure evolution of the whole process was observed by optical and electron microscopes. Results showed that nano-scaled athermal ω phase uniformly precipitated in β matrix of Ti-55511 after rapid solidification, and it had a little reinforcement effects in the remelted layer due to the low contents. After low temperatures aging, ultrafine α lamellas could form in the remelted layer by ω-assisted nucleation. By increasing the aging temperatures, the sizes and volume fractions of α lamellas increase, resulting in an improvement of surface hardness and wear resistance. However, the high surface hardness did not effectively enhance the wear resistance of Ti-55511 due to the ductility deterioration caused by nano-sized α phase of the aged samples. The remelted samples can achieve the highest surface microhardness over 520HV and relatively best wear resistance after aging at 500 °C for 5 h. [ABSTRACT FROM AUTHOR]

Gas tungsten arc welding was used to repair the laser additive manufactured Ti-5Al-5Mo-5V-1Cr-1Fe (Ti-55511) alloy with a subsequent triplex annealing treatment. The tensile properties of heat treated specimens containing of different proportions of weld zone were designed to evaluate the influence of weld zone on tensile properties of the alloy. Microstructures, microhardness and tensile tests were performed to study the mechanical properties and fracture behaviors of the specimens. Results show that dissolved oxygen in the weld zone has a strong influence on increasing the number of α phase nucleation sites that can lead to different α p morphologies in the base metal and weld zone. These different α p can lead to distinct microstructures after triplex annealing treatment but with similar α volume fractions. Besides, plasticity deterioration of the repaired tensile specimens is mainly attributed to the formation of columnar grain boundary α phases in the weld zone which are considered to be the earliest nucleation sites of microcracks and confirmed by in situ tensile test. With the increase of WZ proportions in the cross section of tensile specimens, the plasticity of the alloy gradually decreases. [ABSTRACT FROM AUTHOR]

A novel α+β titanium alloy with multi-alloying addition and low-cost is designed from Ti-6Al-4V. In order to maintain the same [Al] eq and [Mo] eq , the Mo and Zr were added into the alloy instead of V, and the nominal composition of this novel alloy is determined as Ti-6Al-2V-1.5Mo-0.5Zr-0.3Si with a spot of Si added. In this study, a plate of the novel alloy was manufactured by laser additive manufacturing (LAM). The macrostructure, microstructure, compositions, microhardness and room temperature tensile properties of as-deposited alloy were investigated. The results show that the macrostructure of the novel alloy contains large columnar grains and small columnar grains. Compared to the reference alloy Ti-6Al-4V manufactured with the same process, the novel alloy had much finer basket-weave microstructure. This novel alloy, solid-solute with alloying elements Mo, Zr and Si, has higher microhardness and better combination of strength and plasticity compared to Ti-6Al-4V. [ABSTRACT FROM AUTHOR]

The microstructure and mechanical properties of the Ti–6.5Al–3.5Mo–1.5Zr–0.3Si alloy produced by laser melting deposition have been investigated. The columnar grains of the Ti–6.5Al–3.5Mo–1.5Zr–0.3Si alloy due to the layer-by-layer epitaxial growth from the underlying template grains during laser melting deposition, which is roughly parallel to the deposition direction, had been found by optical microscopy; strong 10 1 ¯ 2 α crystallographic texture has been confirmed by X-ray diffraction and electron backscattered diffraction. Depending on the last heating history, the microstructure of the alloy undergoes a continued change opposite to the deposition direction: martensitic α′ (transformed β); coarsened primary α laths with transformed β; coarsened primary α laths; and the fine basketweave microstructure with a few coarsened α laths or annealed martensitic α′. The average Vickers micro-hardness value of the alloy is 364 HV. The alloy parallel to the deposition direction presents lower tensile strength (925 MPa) and better elongation (18.8%), compared with 1025 MPa and 8.2% of that vertical to the deposition direction, which has been discussed using its microstructure characterization. [ABSTRACT FROM AUTHOR]

Abstract: The compositional variation and the microstructural evolution in laser additive manufactured Ti/Ti–6Al–2Zr–1Mo–1V graded structural material were investigated. An anomalous compositional variation and its good correlation with hardness were found. Although, during the forming process, the ratio of Ti–6Al–2Zr–1Mo–1V in feeded powders abruptly changes from 0% to 100%, all the elements exhibit a gradual variation, which is preferred to a graded material because such gradient change can decrease the discontinuity of its microstructures and properties and can remarkably reduce the costs due to the simplified manufacturing process and the rational distribution of materials. [Copyright &y& Elsevier]