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The growing demand for cotton and the low production rate required to meet global demands have encouraged viscose manufacturing from renewable sources. This work develops a sustainable method to extract viscose fibers (cellulosic‐based precursor) from jute, a renewable resource. Jute fiber is the second largest fiber crop in southern Asia, which contains 65%–70% cellulose and contributes to environmental benefits such as oxygen production, carbon dioxide emission, and heavy metal absorption during harvesting. The treated jute fiber was modified to regenerated cellulose (viscose), as confirmed by different characterizations. The Fourier‐transform infrared spectroscopy (FTIR) test 1423, 1365, 1033, and 1021 cm−1 represented that modified jute fiber resembled viscose fiber, and TGA attributed the thermal stability of glass transition below 100°C and thermal degradation to jute viscose fiber. XRD analysis provides a crystal index of 91.79% of viscose from jute fiber, which is higher than the 76.06% crystal index of raw jute. Here, SEM and physiomechanical properties were also characterized by raw jute and viscose from jute fiber. [ABSTRACT FROM AUTHOR]

Vegan leather derived from mushroom mycelium is a revolutionary technology that addresses the issues raised by bovine and synthetic leather. Jute--mycelium-based vegan leather was constructed using hessian jute fabric, natural rubber solution, and extracted polyhydroxyalkanoate (PHA) biopolymer from Bacillus subtilis strain FPP-K isolated from fermented herbal black tea liquor waste. The bacterial strain was confirmed using 16S rRNA genomic sequencing. The structural characteristics of sustainable mycelium vegan leather were identified using FTIR, SEM, and TGA methods. To address the functional features of the developed vegan leather, solubility, swelling degree, WVP, WCA, and mechanical strength were also evaluated. Mycelium networking was further validated by micromorphological examination (SEM) of the leather sample's cross-sectional area. Jute--mycelium leather demonstrated a tensile strength of 8.62 MPa and a % elongation of 8.34, which were significantly greater than the control sample. Vegan leather displayed a strong peak in the O=H group of carbohydrates in the examination of chemical bonds. A highfrequency infrared wavelength of 1,462 cm-1 revealed the amide group of protein due to the presence of mycelium, while the absorption peak at 1,703 cm-1 in leather indicated the crosslinking of PHA. Moreover, the TGA study finalized the thermal stability of leather. The enhanced hydrophobicity and reduced swelling degree and solubility also endorsed the water resistance properties of the leather. The results of the investigation substantiated the potential properties of mycelium vegan leather as animal- and environment-free leather. [ABSTRACT FROM AUTHOR]

The present work was designed to investigate the effect of maceration, ultra-sound, and microwave-assisted extraction on free, esterified, and bound phenolics of Tulaipanji rice (Oryza sativa L.) flour. Antioxidant activity was measured by DPPH, ABTS, SOD, and reducing power assays. HPTLC analysis was performed for identification and quantification of phenolics in different extracts. Total phenolic (TPC) and total flavonoid contents (TFC) were found significantly high (p < 0.05) in microwave-assisted extraction of bound phenolics compared with other methods. Microwave-assisted extracts showed highest DPPH radicals, ABTS radicals, SOD, and reducing power activity. Further, Pearson's correlation study exhibited a significant positive correlation within % yield, TPC, and TFC. Significant negative correlation was found within % yield, TPC, TFC, and antioxidant activity. The study found that extractive value, antioxidant activity, and phenolic contents varied with the extraction methods. Microwave-assisted extraction technique showed the best performance for extraction as compared to other methods. [ABSTRACT FROM AUTHOR]

Black rice ( Oryza sativa L.) is a rich source of phenolics and anthocyanins. It was aimed to investigate the effect of different extraction methods such as conventional solvent extraction, ultrasound-assisted extraction (UAE), and microwave-assisted extraction (MAE) on antioxidant activity and phenolic profiling of black rice free, esterified, and bound phenolics fractions. Spectrophotometric methods were used to evaluate antioxidant activity and HPTLC was used for phenolics profiling. The highest content of % yield, total anthocyanin (TAC), total phenolic (TPC), and total flavonoid (TFC) contents were detected in MAE. It was also observed that antioxidant activity based on DPPH, ABTS, superoxide radical-scavenging and ferric reducing antioxidant power (FRAP) assays showed highest activity in MAE. Eight phenolic compounds were identified and quantified by a validated HPTLC method. MAE showed most abundant phenolic compounds. A significant positive correlation was established between % yield, total phenolic content, and total flavonoid content ( p  < 0.05) where a significant negative correlation was established between % yield, TPC, and TFC with IC 50 of antioxidant activity ( p  < 0.05). Diverse phenolic contents and antioxidant activity were studied with different forms of phenolics with the different extraction methods. It designates that the extraction techniques had effects on the bioactive compounds as well biological properties., (© 2023 Walter de Gruyter GmbH, Berlin/Boston.)