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Jeon et al . (Reports, 29 January 2021, p. 498) reported reversible fluctuations between disordered and crystalline states during nucleation. We argue that the adoption of “magic numbers” for separation of the size range into three parts is misleading when using the sigmoid functions and that their figure 3B was wrongly illustrated. The crystal shape effect was neglected during theoretical analysis.

Low angle dependence single green polystyrene colloidal crystal films were prepared by vertical deposition method using polystyrene microspheres with size of 380 ± 10 nm as raw material and further modified by adding nano-carbon. Without nano-carbon addition, the film showed various colors with changing the angle of incident light under natural light. With nano-carbon addition, saturation and angle dependence of the polystyrene colloidal crystal film were remarkably improved. With 0.01 wt % nano-carbon addition, since the stray light of other wavelengths other than the band gap light was absorbed by the added nano-carbon, the film showed only green color under different angles of incident light, suggesting that the film had low angle dependence. It is significant in the research of color behavior and is helpful to obtain single color polystyrene colloidal crystal film.

The effects of red/blue=3/1 [R/B=3/1(9/3), as control, CK本试验采用发光二极管(LED)精准调控光源环境,以‘改良大龙茄’为试材,在前期探明红/蓝组合光(R/B)=3/1有利于培育茄子壮苗基础上,以R/B=3/1(9/3,CK

Inverse opal zirconia is useful in many ways because of their ability to combine several chemical and physical properties. In this research, polystyrene template was fabricated by self-assembly method and inverse opal zirconia was prepared by colloidal crystal-templating method. The process of preparation of inverse opal zirconia as well as effects on morphology and phase of as-prepared inverse opal zirconia were studied. The results showed precursor ratio of zirconium acetate and methanol, mass ratio of polystyrene templates and precursor and dipping times had remarkable influence on morphology of inverse opal zirconia. When the precursor ratio was 1:1; the mass ratio was 1:15 and dipped once, much better morphology of inverse opal zirconia was obtained. The mass ratio, sintering temperature and holding time had significant effect on crystallization of zirconia. Pure phase zirconia could be obtained when sintered at 600 oC, holding time was 2h and the mass ratio was 1:1. A distinguished single stop band in the visible region of the spectrum and unique structural color were observed in inverse opal zirconia, which will make this material promising candidate for novel pigment.

Using Bi(NO3)3·5H2O and Si(OC2H5)4 as the starting materials, citric acid and polyethylene glycol (PEG)-6000 as the complexing agents, pure Bi2SiO5 powders with good photocatalytic activity were first prepared at low temperature via Pechini sol–gel method. The effect of calcination temperature on the preparation of pure phase as well as the photocatalytic properties was investigated. The thermal analysis and X-ray diffraction results showed that the crystallization temperature of Bi2SiO5 is about 400 °C and pure sample can be obtained at 550 °C. The infrared spectra indicated the pure Bi2SiO5 samples have an Aurivillius-like structure. Furthermore, the as-prepared Bi2SiO5 exhibited efficient photocatalytic activity in the decomposition of Rhodamine B due to a synergistic effect of adsorption and photocatalysis.

Lithium metatitanate (β-Li 2 TiO 3 ) pebbles were fabricated via the modified indirect wet chemistry method. Effect of varied additives, as polyvinyl alcohol, glycerol, and agar on the properties evolution was investigated. The highest density is obtained by adding 2 wt% (weight percent) polyvinyl alcohol, 3 wt% glycerol, and 3 wt% agar, respectively. β-Li 2 TiO 3 pebbles with relative sintered density of 92.4%T.D. (Theoretical Density), the ratio of the intensity of diffraction peak (002) to that of (−133) of about 2.93, about 1.58 mm in diameter, a better sphericity of 1.02, the particle size of 5–6 μm, and the well-developed surface layered structure are successfully fabricated with 3 wt% glycerol. Glycerol is beneficial to improving the properties by other fabrication method as well.

Metastable Bi2SiO5 phase powders were synthesized successfully by Pechini sol-gel method using a simple starting hydro-alcoholic solution consisting of Bi(NO3)3 · 5H2O, TEOS, citric acid, and PEG-6000. The effects of Bi/Si molar ratio, citric acid, and PEG-6000 on the properties of pure Bi2SiO5 powders were investigated. The crystalline phase and fluorescence properties were characterized. The process of Pechini sol-gel method and the effect of purity on fluorescence properties were studied in this paper. X-ray diffraction results illustrate that single phase of Bi2SiO5 can be obtained at 650°C for 1 h. Furthermore, the maximum fluorescence emission wavelength of the powders is located at 355 nm, which represents the band gap of Bi2SiO5 powders is 3.49 eV.

To get optimal nitrogen (N), phosphorus (P本试验采用三因子二次饱和D-最优设计(310),以蛭石为栽培介质,建立了以氮、磷、钾浓度为变量因子,茄子产量和品质为目标函数的三元二次数学模型,以期得到茄子优质高产最优氮磷钾浓度范围.对模型解析结果表明: 氮、磷、钾浓度对茄子产量和品质均有显著影响.对产量和品质的影响程度均以钾浓度较大,对产量的影响程度以氮浓度次之,磷浓度较小,对品质则为磷浓度次之,氮浓度较小.氮磷、氮钾、磷钾浓度交互对茄子产量均有显著影响;氮钾浓度交互对茄子品质亦有显著影响.在低水平条件下,茄子产量和品质均随氮、磷、钾浓度增加而增加,但超过一定范围后,茄子产量和品质均随之降低.通过计算机模拟运算得出,本试验条件下茄子单株产量达3600 g的施肥方案为:氮16.0～20.0 mmol·L

Due to the increasing number of service agreements between service providers and users and the lack of standard in agreement specifications in service computing environments, there is need for an efficient service mapping and provider selection approach that focuses on Service Level Agreement (SLA) documents. This paper proposes a novel SLA mapping and provider selection approach with annotated ontological semantic information to WS-Agreement and advanced mapping rules using semantic web rule language (SWRL) and web ontology language (OWL) ontologies. The experimental data shows that our proposed approach is superior to other proficient approaches, because it can properly exploit ontological semantic technology in service specification and matchmaking.

Enteropathy-associated T-cell lymphoma (EATL) is a rare gastrointestinal non-Hodgkin's lymphoma, originating from intraepithelial T-lymphocyte, which is specifically associated with celiac disease. EATL most commonly presents in the sixth and seventh decades of life. We report a unique case of type I EATL in the colon with liver metastasis, which was presented with nonspecific radiological findings and at a very young age (29 years old) compared with previously published data. We suggest that EATL should be regarded as part of differential diagnosis in any patient presenting with abdominal pain, diarrhea, weight loss, and malabsorption because delay in treatment can result in an irreversible clinical outcome.

The solution culture method was used to study the effects of sodium nitroprusside (SNP) on plant growth, nutrient uptake and antioxidant enzyme activities of tomato seedlings under iron deficiency and NO采用营养液培养方法,研究外源NO供体(硝普钠,SNP)对缺铁和硝酸盐胁迫番茄幼苗生长、养分吸收及抗氧化酶活性的影响.结果表明: 处理7 d后,缺铁使番茄幼苗生长受到抑制,叶绿素a、b、类萝卜素含量显著降低,出现明显失绿症状;降低叶片中超氧化物歧化酶(SOD)、过氧化物酶(POD)和过氧化氢酶(CAT)的活性,电解质渗漏率、丙二醛含量明显增加,脯氨酸和可溶性糖含量变化不显著,幼苗叶片和根中N、P、K、Ca、Mg、Fe含量比对照处理有不同程度的减少.硝酸盐和缺铁双重胁迫对番茄幼苗生长抑制加剧,叶绿素a、b、类萝卜素含量、SOD、POD和CAT活性显著降低,电解质渗漏率、脯氨酸、可溶性糖和丙二醛含量明显增加;番茄幼苗叶片和根中N、P、Mg、Fe含量显著减少,而K、Ca含量显著增加. 与不添加处理相比,添加0.1 mmol·L

'Jinyan No. 4'cucumber was used as experimental material. The growth of cucumber radicles treated with different concentrations of p-hydroxybenzoic acid (0, 2.5, 5, 7.5, 10, 12.5, 15, 17.5 and 20 mmol·L以‘津研四号’黄瓜为试材,分别用0、2.5、5、7.5、10、12.5、15、17.5、20 mmol·L

To investigate the effect of calcium and ABA on photosynthesis and the activities of antioxidant enzymes in cucumber seedlings under drought stress, the cucumber was used as the expe-riment materials, normal nutrient solution culture was considered as the control, and PEG-6000 application in the nutrient solution simulated the drought stress. There were five different treatments which were spraying water, ABA, CaCl为探讨在干旱胁迫下钙与脱落酸对黄瓜幼苗光合作用及相关酶活性的影响,以黄瓜为试材,正常营养液栽培为对照,利用PEG-6000(聚乙二醇)营养液添加模拟干旱胁迫,设干旱胁迫条件下幼苗叶片喷施清水、脱落酸(ABA)、CaCl

The effects of white light, red light, blue light, yellow light, red+blue light and red+blue+yellow light on the growth and quality of Gynura bicolor were investigated under the same light intensity (350±5 μmol·m以紫背天葵为供试材料,采用LED灯精量调控光质和光强,研究相同光照强度(350±5 μmol·m

In breast cancer, metastasis is the main reason for patient mortality. In the present study, we used breast cancer MDA-MB-231 cells and a mouse xenograft model to demonstrate the effect of emodin on the migration, invasion and metastasis of human breast cancer MDA-MB-231 cells and the related mechanisms. In vitro, wound healing and Transwell assays showed that emodin dose-dependently inhibited the migration and invasion of MDA-MB-231 cells. Enzyme-linked immunosorbent assay (ELISA) showed that emodin decreased the secretion of MMP-2 and MMP-9. Western blot analysis showed that emodin downregulated the expression levels of MMP-2, MMP-9, uPA and uPAR as well as p38 inhibitor SB203580 and ERK inhibitor PD980559, even though TIMP-1 and TIMP-2 were not obviously changed in the MDA-MB-231 cells. Furthermore, emodin inhibited the activity of p38 and ERK1/2 in the MDA-MB-231 cells. In vivo, emodin inhibited lung metastasis in mice bearing the breast cancer MDA-MB-231 xenografts with no obvious changes in body weight, liver and kidney functions. These results indicated that emodin inhibited the lung metastasis of human breast cancer in a mouse xenograft model, and inhibited the invasion of MDA-MB-231 cells associated with the downregulation of MMP-2, MMP-9, uPA and uPAR expression as well as decreased activity of p38 and ERK.

The new method of laser prestressed bending of Titanium alloy sheet is put forward in this paper. Titanium alloy sheet is produced pre-deformation by a clamp, the laser beam with some certain intensity scans its surface along the given path, and it is formed due to the thermal effect of the laser to reduce the yield strength of the scanning area and enhance its plastic deformation ability. A feasibility experiment for Ti-6Al-4V sheet is done and the bending effect is remarkable. Laser prestressed bending mechanism is described and the main influence factors are analyzed.

Bi2SiO5 is a metastable phase compound and one of the important Bi-based Aurivillius phase oxide semiconductors. Pure Bi2SiO5 powders were synthesized successfully by Pechini sol–gel method. The samples were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, field-emission scanning electron microscopy, transmission electron microscopy, thermal analyzer, FTIR spectrometer, Raman spectrometer, fluorescence spectrophotometer and UV/Vis/NIR spectrophotometer. The mechanism of the reaction process was studied. The structure, the optical and photocatalytic properties of pure samples were investigated. The results show that citric acid, polyethylene glycol, solvents and calcination temperature have important effects on the reaction, and pure Bi2SiO5 can be obtained at 650 °C for 1 h. The as-prepared Bi2SiO5 has a typical Aurivillius-like structure and its bang gap energy is 3.5 eV. The results of degradation of Rhodamine B reveal that pure Bi2SiO5 powders prepared by Pechini sol–gel method possess a synergistic effect of adsorption and photocatalysis, which indicates that the Bi2SiO5 powders can be used as an efficient material for wastewater treatment.

Pure eulytite Bi4(SiO4)3crystals were prepared by high temperature melt cooling method using Bi2O3and SiO2as starting materials. In this study, the properties of the samples were characterized by thermo gravimetric (TG),differential scanning calorimeter (DSC), field-emission scanning electron microscopy (FESEM) and X-ray diffraction (XRD). The results showed that eulytite Bi4(SiO4)3was crystallized when high temperature glass-melt were cooled to 943°C and obvious exothermal peak is shown on the DSC curve; and pure eulytite Bi4(SiO4)3crystals were synthesized by keeping the processing temperature for 8 hours. Bi4(SiO4)3grains grew larger and the amount of vacancy increased along with the extension of holding time, while Bi4(SiO4)3grains still presented a structure of partial ordering. Eulytite Bi4(SiO4)3prepared through melt-cooling method is of high purity and good stability, and can be applied as starting materials of preparation of Bi4(SiO4)3thin film and high quality Bi4(SiO4)3macrocrystal.

The sound transmission loss (STL) of the acoustic parts in the vehicle was proposed to be computed using the Sound Pressure Level measured at the several locations inside the vehicle and the transmitted Sound Intensity Level on the vehicles exterior panel, which the acoustic treated vehicle passenger compartment is assumed as a small reverberation room. The necessary parts retrofits and acoustic treatments for Sound transmission loss tests of the acoustic parts in the vehicle were listed. The values of the appropriate number and positions of the loud speakers, microphones and sound intensity probes for Sound transmission loss of the acoustic parts in the vehicle were recommended. The in vehicle sound transmission loss tests of the acoustic parts such as the doors, carpets, wheel house etc. were achieved in the semi-anechoic room. Based on the door system, the correlation work has been done among the methods of the proposed in vehicle STL test, the reverberation - semi-anechoic chamber buck STL test and SEA analysis.

In this paper, an experimental study on the powertrain in vehicle sound power test was presented. The necessary parts retrofits and acoustic treatments for the powertrain sound power test in the vehicle were listed. The criteria and correction method of the appropriate background noise level for the powertrain sound power level test in the vehicle were discussed. The powertrain sound power tests in the vehicle were achieved in the low noise chassis Dynamometer in the semi-anechoic chamber. Based on the test results, the acoustic component contributions for the powertrain sound power levels were given .

Harmonic components in holospectrum are mainly due to the lateral vibration, and they are important parameters in fault diagnosis of rotating machinery. However, defects on measuring shaft surface are also included in harmonic components in holospectrum and may lead to misdiagnosis. It’s necessary to study a method to identify the shaft surface defects. Based on the manufacturing process of outer round, this paper studies the forming mechanism of harmonic defects on outer round and their characteristics in holospectrum. An experimental example is also given to validate the theoretical analysis, and the results show that holospectrum can recognize the harmonic defects on outer round well.

Metastable crystal Bi2SiO5 has significant properties including dielectric, thermoelectricity and nonlinear optical properties. Metastable crystal Bi2SiO5 has been successfully prepared by melt cooling method in this study. Surface tension of high-temperature melt Bi2SiO5 was measured by Suspension method; metastable crystal Bi2SiO5 construction was assigned by IR(Infrared Radiation). The experimental result showed that Bi2SiO5 flux density decreased with the increasing temperature in 830-1095°C range; surface tension changed quadratic with the decreasing temperature. The [SiO4]4- anions of Bi2SiO5 originated from the isolated [SiO4] tetrahedron in the glass to a chain connected structure.

Metastasis is the major cause of death in breast cancer patients. In this study, we investigated the effects of baicalin, a natural compound, on cell migration, invasion and metastasis using human breast cancer MDA-MB-231 cell line as model system. Baicalin not only dose-dependently inhibited MDA-MB-231 cells migration and in vitro invasion, but also suppressed the tumor outgrowth and the pulmonary metastasis of MDA-MB-231 cells in xenograft model. Importantly, treatment of baicalin caused little change in body weight, liver and kidney function of recipient animals. Tumorigenesis-inhibitory effect is likely linked to the capability of baicalin to downregulate metalloproteinase (MMP)-2, MMP-9, urokinase-type plasminogen activator (uPA) and uPA receptor (uPAR) expression in MDA-MB-231 cells. As baicalin blocked p38 mitogen-activated protein kinase (MAPK) activity and treatment of p38MAPK inhibitor SB203580 led to the reduction of MMP-2, MMP-9, uPA and uPAR expressions, we concluded that baicalin suppresses the tumorigenecity of MDA-MB-231 cells by down-regulating MMP-2, MMP-9, uPA and uPAR expressions through the interruption of p38MAPK signaling pathway.

Breast cancer remains the leading cause of cancer-related deaths among women. Owing to high efficiency and low toxic effects, further exploration of natural compounds from Chinese herbal medicine may be an efficient approach for breast cancer drug discovery. In this study, we investigated the effects of evodiamine on the growth and metastasis of MDA-MB-231 human breast cancer cells in vitro and in vivo. In vitro, evodiamine inhibited cell migration and invasion abilities through downregulation of MMP-9, urokinase-type plasminogen activator (uPA) and uPAR expression. Evodiamine-induced G0/G1 arrest and apoptosis were associated with a decrease in Bcl-2, cyclin D1 and cyclin-dependent kinase 6 (CDK6) expression and an increase in Bax and p27Kip1 expression. Moreover, evodiamine regulated p-ERK and p-p38 MAPK expression. Evodiamine-induced apoptosis was enhanced by its combination with the extracellular signal-regulated kinase (ERK) inhibitor PD98059 or the p38 mitogen-activated protein kinase (p38 MAPK) inhibitor SB203580. Evodiamine-inhibited metastasis was partly blocked by combination with PD98059 or SB203580. In vivo, the administration of evodiamine (10 mg/kg) significantly reduced tumor growth and pulmonary metastasis. These results demonstrate that evodiamine possesses antitumor activities via inhibition of cell migration and invasion, arrest of the cell cycle and induction of cell apoptosis in MDA-MB-231 cells.

In this article, Bi2SiO5 powders were prepared by molten salt method. Via uniform experiment, the effects of various technological parameters (sintering temperature, holding time, excessive contents of Bi2O3 by weight, and ratios of salts) on synthesis of Bi2SiO5 powders were investigated using X-ray diffraction (XRD), scanning electron microscopy (SEM), and thermal analysis. Forming mechanism of sheets was discussed. According to the analysis of XRD and SEM, the sample mainly contains Bi2SiO5 phase when the temperature is 650°C, holding time is 2.5 h, excessive content of Bi2O3 is 5 wt%, and the ratio of salts is 50 wt%. Interface reacting mechanism can be used to explain the coarsening process of bismuth silicate sheets produced in molten salt synthesis. In addition, dissolution–precipitation mechanism also plays an important role in the synthesis of bismuth silicate sheets.

The bismuth silicate powders were prepared by reaction of Bi2O3 and SiO2 as raw materials in KCl-K2CO3, NaCl-Na2CO3, K2CO3-Na2CO3, KCl-NaCl, NaCl-Na2SO4, and KCl-K2SO4 molten salts. Pure Bi12SiO20 powders were synthesized in KCl-K2CO3 flux at 635°C for 1 h, which was lower than that of conventional solid state reaction. X-ray diffraction reveals that the phases of the samples are different in various molten salts. Only Bi12SiO20 phase can be observed in the molten salts with ions. However, a mixture of Bi12SiO20, Bi2SiO5, and Bi4Si3O12 phase are observed in the molten salts without ions. Therefore, the carbonates are not only used as the flux and reaction medium, but also inhibit the formation of other bismuth silicates in the synthesis of Bi12SiO20 powders by molten salt synthesis. The scanning electronic microscopy image indicates that the mechanism of molten salt synthesis in the case of KCl-K2CO3 and NaCl-Na2CO3 are “dissolution-precipitation mechanism.” UV-Vis spectra reveals the absorption edge for ...

In this work, barium titanate (BaTiO3) powders were synthesized via two Pechini sol-gel processes using citric acid and polyethylene glycol-6000 as chelating agents. Attempts had been made to understand the thermal behavior of the polymeric intermediates with the help of thermogravimetry-differential scanning calorimetry (TG-DTG-DSC) thermograms. The structural coordination of as-prepared polymeric intermediates was investigated by Fourier transform infrared (FTIR) analysis. The phase and structure of the powders calcined at different temperatures were characterized by X-ray diffraction (XRD) and field emission scanning electron microscope (FE-SEM). Preparation of the polymeric precursors can influence the mechanism of the BaTiO3 synthesis. The formed intermediate phase BaCO3 appears in gel-2 system, and BaCO3 phase does not disappear at 720°C. The formed intermediate phases of gel-1 differ from that of gel-2. The intermediate phases of gel-1 are anatase TiO2 and rutile TiO2, and the intermediate phase Ba...

Polyaniline nanorods, nanoplates and urchin-like structures have been synthesized successfully by the template-free method of aniline and peroxo–polytungstic acid using ammonium persulphate as the oxidant in aqueous solution. The peroxo–polytungstic acid concentration and reaction temperature play important role in the formation process of polyaniline nanostructures. As the precursor concentration increased to 0.29mol/L, nanorods and urchin structures were obtained. With the decrease of temperature, the amount of PANI nanoplates with radially aligned dendritic surface structures will increase. The radially aligned dendritic surface is probably due to the molecular structures of the dopant, the linear nature of PANI chains and the second nucleation formation.

The effects of red light, blue light, red+blue light and white light (control) generated by LED on the quality and antioxidation capacity of fruit and yield of ' Brita' eggplants were stu died. The results showed that under blue LED, the soluble protein, free amino acids contents o eggplant pulps and the anthocyanin content of eggplant peels were significantly higher by 15.1%, 27.2% and 73.6% than control respectively, but flavonoid and phenolic contents of pulps and the yield were significantly lower than those of the other treatments. Under red LED, the eggplant peels flavonoid was remarkably increased, but vitamin C (Vc) and soluble protein contents were consi derably decreased. Under red+blue LED, the soluble sugar of pulps and phenolic, red pigment yellow pigment contents, total antioxidation capacity (TAG) of peels and the yield were significantly higher than those of the other treatments, in which, the TAC of peels and the yield increased by 43.5% and 43.4% compared with control, respectively. Vc, flavonoid and phenolic contents and TAC of eggplant pulps were the highest under white LED. There was significant positive correlation between the phenol content of peels and Vc content of pulps with TAC. Under the protected cultivation condition, an appropriate amount of blue or red LED could improve the quality of eggplant fruit, and red+blue LED was more beneficial to promote the quality of eggplant peels and the yield.

In this paper, Bismuth silicate (Bi4Si3O12, BSO) powders were prepared by reaction in molten salts (NaCl and KCl) using Bi2O3 and SiO2 powders as raw materials. The effects of salt contents and excessive contents of Bi2O3 and SiO2 were characterized by X-ray diffraction and scanning electron microscopy. The properties of Bi4Si3O12 powders were analyzed via fluorescence spectroscopy. Forming mechanism of platelets was discussed. The experimental results suggest that Bi4Si3O12 powders are produced at 780 °C for 4 h with 40 wt% salts and 5 wt% excessive content of Bi2O3. The peaks of excitation spectrum and emission spectrum for BSO powders are separately located at 266 and 457.6 nm. Compared with crystal materials, the excitation spectrum and emission spectrum of Bi4Si3O12 powders indicate blue shift. Interface reacting mechanism can be used to explain the coarsening process of bismuth silicate platelets produced in molten salt synthesis. In addition, dissolution–precipitation mechanism also plays an important role in the synthesis of bismuth silicate platelets.

Poly (aminohexylaminomethyl/phenyl) silsesquioxane (PAHAMPSQ) microparticles with diameter of 350 nm were synthesized by the hydrolytic condensation of aminohexylaminomethyltriethoxysilane (AHAMTES) and phenyltriethoxysilane (PTES) in the presence of H2O by using tetraethylammonium hydroxide (TEAOH) catalysts. PAHAMPSQ containing both aminohexylaminomethyl and phenyl groups were confirmed from FT-IR, TGA. XRD patterns indicate that a certain ordered structure existed in PAHAMPSQ molecules. Contents of amino of PAHAMPSQ were determined by elemental analysis. SEM images show both granular and flake exist in PAHAMPSQ microparticles. Yield of PAHAMPSQ in different AHAMTES/PETS molar ratios was about 80%. PAHAMPSQ offers the potential utility as building blocks for divers and novel organic/inorganic materials.

In this paper, Ni0.5Zn0.5Fe2O4ferrite ceramics were produced with Ni0.5Zn0.5Fe2O4powders prepared by reaction in a molten salt using Fe2O3, NiO and ZnO powders as raw materials. Ni-Zn powders were characterized by X-ray diffraction (XRD). Density and shrinkage in diameter of Ni0.5Zn0.5Fe2O4ceramics were measured. MicroSubscript text structures were observed using field emission scanning electron microscopy (FESEM), and magnetic properties were examined by HP4291B impedance analyzer. XRD pattern indicated that the powders synthesized at 900°C for 1h were pure spinel Ni0.5Zn0.5Fe2O4phase. Via the measurement of density and shrink in diameter, optimal temperature was 1200°C and holding time was 2h, which was in accord with the results concluded from micrographs. FESEM images illustrated that the average grain size increased with increasing holding time, which followed the Ostwald liquid growth mechanism. At lower frequencies, the initial permeability (μi) increased from 86.65 to 183.48 with increasing holding time, while the threshold frequency decreased from 13.3MHz to 8.52MHz, which implied the initial permeability (μi) variation complied with the Snoek law to some extent.

Polyaniline/SiO2 composites were prepared by the SiO2 particles whose surface character was modified by succinic acid. The composites were characterized by Fourier transform infrared (FT–IR) spectroscopy, X–ray diffraction (XRD), thermogravimetric analysis (TGA), scanning electron microscope (SEM). The results demonstrated that the thermal stability of PANI had improved.

α-Al2O3platelets were prepared in the interface of Na2O-CaO-SiO2glass induced by Al. The morphology of the platelets was observed by Environmental Scanning Electron Microscopy (ESEM). The platelets are irregularly shaped at 720°C for 30mins and share mean thickness of 200nm. EDS shows that the platelets are rich in Si, reasonably due to the formation of Al-Si eutectic. At 1200°C, the prepared platelets have mean diameters between 400nm and 1000nm, most of which are aggregated and part through intergrowth. The crystals develop from the glass and can form good moistening with the glass matrix.

Hydroxyapatite (HA) was synthesized in presence of 20wt% m-ZrO2by solid state reaction between tricalcium phosphate(TCP) and Ca(OH)2at 1000 °C for 2h. Similarily, Fluorine hydroxyapatite(FA) was synthesized using tricalcium phosphate and calcium fluoride as raw materials at 1000 °Cfor 3h. The as-prepared HA was mixed with 10%,25%,45%,55%,70wt% FA and the mixture was sintered at 1000°C-1400°C for 2h. The main phase and bulk density was measured. The results show that when the relative amount of FA to HA increased, the decomposition of the composite is decreased gradually because of the formation of thermally stable FHA solid solutions. Low temperature would effect the exchange of ionic between FA and HA,while high temperature would impact synthesis of composites, because high temperature would lead to dissolution of HA ,which has to react with FA. Increase the content of HA would be advantage for synthesis FHA-ZrO2composite.

α-Al2O3 platelets were prepared in the interface of Na2O-CaO-SiO2 glass induced by Al. Phase identification was accomplished by X-ray diffraction analysis. The morphology of the platelets was observed using an Environmental Scanning Electron Microscopy (ESEM). The changes for the mixtures of the Al powders and the glass powders that occurred during heating were characterized by a combination of differential scanning calorimetry (DSC) and thermalgravimety(TG) on a multi-functional instrument. Confirmed by XRD and ESEM, at 1200°C, the prepared platelets have mean diameters between 400nm and 1000nm. Most of them are aggregated and part of them through intergrowth. The crystals develop from the interface between glass and Al, and can form good moistening with the glass matrix. DSC/TG shows that γ-Al2O3 formed by oxidation of Al, transforms into α-Al2O3 and grow into the platelet α-Al2O3 crystals owing to the molten Al and the molten glass. On the other hand, part of the molten Al erodes into the glass and makes the deviation of the Na2O-CaO-SiO2 ternary system into Na2O-Al2O3-SiO2 ternary system, resulting in the formation of NaAlSiO4.

Pure Bi12SiO20powder was successfully prepared by a molten salt method using Bi2O3and SiO2as raw materials and using KCl-K2CO3as flux at 635°C with the heating rate of 5°Cmin-1. The phase composition and microstructure of these products were analyzed by X-ray diffraction and scanning electron microscopy, and the effects of the processing parameters, such as the ratio of Bi2O3/SiO2, calciniation temperature, isothermal time and relative amount of salt, on the composition and particle size were investigated. The results indicated that regardless of changing the ratio of Bi2O3/SiO2, calciniation temperature, isothermal time or relative amount of salt the reaction only yielded Bi12SiO20without Bi2SiO5and Bi4Si3O12. Henceforth, KCl-K2CO3molten salts may be considered as an ideal reaction medium to synthesize pure phase of Bi12SiO20. The particle size of Bi12SiO20phase can be determined by changing the temperature, isothermal time and relative amount of salt.

Many automobile security systems are provided today, but their functions are not enough to satisfy the applications for Environmental Monitoring based on Service Oriented Architecture (SOA).In this paper, we proposed and introduced new device which is an automobile information Identification device with sensors network to strengthen automobile security system function for monitoring environment. This device aims at monitoring status of automobile as well as its environment by collecting data through sensors network. In order to increase the security, we used a new designed architecture of sensors network to gather data. GPS and GPRS were also added to locate the automobile and to transmit filtered data into the monitor. A New Design approach of system was discussed on both software and hardware. One math model for showing gas and voltage value relation was established. In order to improve system reliability, various testing methods were applied in this system. The results showed that the combination of average filtering algorithm and median filtering algorithm to inhibit interference signal at variety of frequency case can effectively filter different frequency interference signal in the software system. The advantage of this system was discussed. The system has low cost, high performance, real-time and reliability characteristics. It can not only strengthen current security system functions but also can satisfy requirements of future automobile. It also has large potential market.

Based on ARM,multifuncttion GPS/GPRS automobile security system was designed,which focused on security and detectiong.The system combines with detection technology, sensor technology, GPS technology, GPRS technology and digital filtering technology.This system was discussed from software and hardware. Related math model was established. Corresponding test was been brought forward to improve system reliability. Average filtering method and median filtering algorithm have been used to inhibiting interference signals with variety of frequency in software. In this paper,the advantages of this system have been discussed.The embeded system realizes the function with characteristics of low cost, high performance, real-time and reliability ,it has high practical value.

The control effects of Eupolyphaga (Eupolyphaga sinensis Walker) frass and its extracts on Meloidogyne incognita were studied through laboratory assays and pot experiments, and the organic volatile compounds and oligochitosan contents in the frass were analyzed. The results indicated that the nematode immobility and mortality was significantly increased with increasing the extract concentration and treatment time. Compared with the control, egg hatching was significantly inhibited when the extract concentration was beyond 20%. Pot experiment indicated that root galling of tomato seedlings was reduced and the relative control effect was significantly improved with the increasing frass application. Meanwhile, plant height, stem diameter and leaf number of tomato increased with the increasing dosage of eupolyphaga frass. The ingredients analysis showed that the content of oligochitosan was about 4.35% and there were 9 categories and 110 kinds of volatile compounds in the frass.